A compound of N- nitro-2,4,6-trifluoroaniline, synthesis method and application thereof
A technology of trifluoroaniline and compound is applied in the field of compound N-nitro-2, and achieves the effects of simple process, few steps and low cost
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Embodiment 1
[0027] The synthetic method of compound N-nitro-2,4,6-trifluoroaniline comprises the following steps:
[0028] (1) Add 40ml toluene, 11.77g (0.08mol) 2,4,6-trifluoroaniline (purchased from Changzhou Yetai Fine Chemical Industry Co., Ltd. Research Institute), water bath temperature control 20 ℃, magnetic stirring, slowly dropwise add a mixture of 6ml of fuming nitric acid with a concentration of 98% and 10ml of toluene, the dropwise addition is completed in 20 minutes, continue to stir for 30 minutes, and stop the reaction. Suction filtration under reduced pressure, washing with 10ml of toluene to obtain a white powder solid, namely 2,4,6-trifluoroaniline nitrate, vacuum drying, the yield was 96%;
[0029] (2) Add 100ml toluene, 10.5g (0.05mol) 2,4,6-trifluoroaniline nitrate in a 250ml three-necked flask equipped with magnetic stirring, thermometer, constant pressure dropping funnel and reflux condenser, and control the temperature at 25 -30°C, slowly add a mixture of 8ml acet...
Embodiment 2
[0037] Test of Plant Growth Regulatory Activity of Compound N-nitro-2,4,6-trifluoroaniline
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