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Method for improving freeze-drying survival rate of Lactobacillus acidophilus

A technology of Lactobacillus acidophilus and survival rate, applied in the direction of microorganism-based methods, biochemical equipment and methods, bacteria, etc., can solve the problems of low number of viable bacteria and low survival rate of freeze-drying

Inactive Publication Date: 2014-07-09
SHAANXI RES INST OF AGRI PRODS PROCESSING TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The object of the present invention is to provide a method for improving the freeze-drying survival rate of Lactobacillus acidophilus, which can solve the problems of low freeze-drying survival rate and small number of viable bacteria in the freeze-drying process of Lactobacillus acidophilus

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1-1

[0019] Sterilize the MRS broth at 118°C for 15 minutes, cool it to room temperature, and then inoculate Lactobacillus acidophilus at 4% (V / V) inoculum, culture at 37°C for 18 hours, and then place the culture solution at 9°C for 1.0 h, take a sample to measure the number of viable bacteria, then centrifuge at 4°C, 7000 rpm for 10 min, discard the supernatant to obtain Lactobacillus acidophilus sludge, weigh the sludge, and add 20% (W / W) skim milk of the sludge weight Powder, then add 80% (W / W) phosphate buffer of pH 6.8 to the weight of bacteria mud, then pre-freeze at -40°C for 8 hours, and then place it in a freeze dryer for lyophilization, 4-6Pa, -50 Freeze-drying at ℃ for 24h, you can get Lactobacillus acidophilus powder, the freeze-drying survival rate is 70.45% (control group is 46.11%), the number of viable bacteria is 2.1×10 11 cfu / g((The control group is 1.10×10 11 cfu / g)).

Embodiment 1-2

[0021] Sterilize the MRS broth at 118°C for 15 minutes, cool it to room temperature, and then inoculate Lactobacillus acidophilus at a 4% (V / V) inoculum, culture at 37°C for 18 hours, and then place the culture solution at 8°C for 0.5 h, take a sample to measure the number of viable bacteria, then centrifuge at 4°C, 7000 rpm for 15 minutes, discard the supernatant to obtain Lactobacillus acidophilus sludge, weigh the sludge, and add 10% (W / W) weight of the sludge with skim milk Powder, then add 90% (W / W) phosphate buffer solution of pH 6.8 with the weight of bacteria mud, then pre-freeze at -40℃ for 12h, then put it in a freeze dryer for lyophilization, 6Pa, -60℃ Lyophilize for 21h to obtain Lactobacillus acidophilus powder.

Embodiment 1-3

[0023] Sterilize the MRS broth at 118°C for 15 minutes, cool it to room temperature, and then inoculate Lactobacillus acidophilus at a 4% (V / V) inoculum, culture at 37°C for 18 hours, and then place the culture solution at 10°C for 1.5 h, take a sample to measure the number of viable bacteria, then centrifuge at 4°C, 7000 rpm for 11 minutes, discard the supernatant to obtain Lactobacillus acidophilus sludge, weigh the sludge, and add 16% (W / W) skim milk of the sludge weight Powder, then add 84% (W / W) phosphate buffer solution of pH 6.8 with the weight of bacteria mud, then pre-freeze at -40℃ for 11h, then put it in a freeze dryer for lyophilization, 4Pa, -52℃ Lyophilize for 18h to obtain Lactobacillus acidophilus powder.

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PUM

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Abstract

The invention aims to provide a method for improving the freeze-drying survival rate of Lactobacillus acidophilus. The method comprises the following steps of: culturing the Lactobacillus acidophilus for 18h at the temperature of 37 DEG C, performing sublethal treatment on the Lactobacillus acidophilus, centrifuging for 10 to 15min at the temperature of 4 DEG C at the rotating speed of 7,000rpm, adding skimmed milk and a phosphate buffer solution into bacterial sludge of the Lactobacillus acidophilus, pre-freezing for 8 to 12h at the temperature of -40 DEG C, and putting into a freeze dryer and freeze-drying for 18 to 24h at the temperature of between -50 and -60 DEG C under the vacuum degree of between 4 and 6Pa to obtain bacterial powder of the Lactobacillus acidophilus. In the method for improving the freeze-drying survival rate of the Lactobacillus acidophilus, a Lactobacillus acidophilus culture solution is subjected to cold shock, heat shock or acid shock treatment first so as to ensure that the Lactobacillus acidophilus induces to synthesize cold shock protein and heat shock protein under adverse circumstances or changes the composition of fatty acid of cell membranes, so that the resistance of the Lactobacillus acidophilus in the subsequent freeze-drying process is improved, and the freeze-drying survival rate and the viable count of the bacterial powder are improved.

Description

Technical field [0001] The invention belongs to the technical field of production of Lactobacillus acidophilus products, and relates to a method for improving the lyophilized survival rate of Lactobacillus acidophilus. Background technique [0002] Lactobacillus acidophilus (Lactobacillus acidophilus) belongs to the genus of Lactobacillus in the Lactobacillus family. It has a slender rod shape, and the cell size is generally 0.6~0.9*1.5~6.0μm. It is single, double or 2-3 short Chain arrangement. No flagella, no exercise, Gram staining positive, facultative anaerobic, naturally present in human and animal gastrointestinal tract, human oral cavity, vagina and traditional fermented milk. The optimum growth temperature is 35℃~38℃, no growth below 20℃, and the highest growth temperature is 43℃~48℃. It has poor heat resistance and can use glucose, fructose, lactose and sucrose for homogenous fermentation to produce DL lactic acid. [0003] Lactobacillus acidophilus is one of the common...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C12N1/20C12N1/04C12R1/23
Inventor 舒国伟王娟陈合马齐秦涛张华张强
Owner SHAANXI RES INST OF AGRI PRODS PROCESSING TECH