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Silicon carbide ceramic product and preparation method

A silicon carbide ceramic and silicon carbide technology, which is applied in fire-resistant coatings and other directions, can solve the problems of easy damage to equipment parts, high equipment maintenance costs, and generally expensive construction costs, so as to achieve easy industrialization, high production efficiency, and improved corrosion resistance. Effect

Active Publication Date: 2013-07-03
SINOSTEEL LUOYANG INST OF REFRACTORIES RES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The cost of high-temperature sintering equipment with an operating temperature above 2000°C is generally more expensive
In addition, equipment components are easily damaged when operating at high temperatures, the cost of components is also high, and the maintenance cost of equipment is also high

Method used

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  • Silicon carbide ceramic product and preparation method
  • Silicon carbide ceramic product and preparation method
  • Silicon carbide ceramic product and preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] (1) Ingredients: Calculated according to mass percentage, the specific composition ratio is shown in Table 1.

[0021] Table I

[0022]

[0023] Accurately weigh the above raw materials according to Table 1, with an accuracy of 0.1g. Put the weighed silicon carbide powder, silicon carbide powder, B 4 C micropowder is kneaded in a planetary ball mill for 30 minutes to prepare a mixed fine powder. Then mix the silicon carbide particles in the mixer for 5 minutes, add the binder, mix for 5 minutes, and finally add the mixed powder, and mix for 15 minutes to ensure that the materials have been mixed.

[0024] (2) Forming: The mixed materials are pressed into a pre-defined size blank by a forming machine.

[0025] (3) Drying: The molded body is placed in a drying equipment, and the temperature is slowly raised at a rate of 1°C / min. The temperature is raised to 200°C and then kept for 8 hours.

[0026] (4) Sintering: Put the dried green body in a silicon carbide smelting furnace, and...

Embodiment 2

[0030] (1) Ingredients: Calculated according to the mass percentage, the specific composition ratio is shown in Table 2.

[0031] Table II

[0032]

[0033] Accurately weigh the above raw materials according to Table 1, with an accuracy of 0.1g. Put the weighed silicon carbide powder, silicon carbide powder, B 4 C micropowder is kneaded in a planetary ball mill for 30 minutes to prepare a mixed fine powder. Then mix the silicon carbide particles in the mixer for 5 minutes, add the binder, mix for 5 minutes, and finally add the mixed powder, and mix for 15 minutes to ensure that the materials have been mixed.

[0034] (2) Forming: The mixed materials are pressed into a pre-defined size blank by a forming machine.

[0035] (3) Drying: The molded body is placed in a drying device, and the temperature is raised at a rate of 1°C / min. After the temperature is raised to 200°C, it is kept for 8 hours.

[0036] (4) Sintering: Put the dried green body in a silicon carbide smelting furnace, and ...

Embodiment 3

[0040] (1) Ingredients: Calculated by mass percentage, the specific composition ratio is shown in Table 3.

[0041] Table Three

[0042]

[0043] Accurately weigh the above raw materials according to Table 1, with an accuracy of 0.1g. The weighed silicon carbide fine powder, silicon carbide fine powder, and B fine powder are kneaded in a planetary ball mill for 30 minutes to prepare mixed fine powder. Then mix the silicon carbide particles in the mixer for 5 minutes, add the binder, mix for 5 minutes, and finally add the mixed powder, and mix for 15 minutes to ensure that the materials have been mixed.

[0044] (2) Molding: The mixed materials are pressed into a product of predetermined size with a molding machine.

[0045] (3) Drying: The molded body is placed in a drying device, and the temperature is raised at a rate of 1°C / min. After the temperature is raised to 200°C, it is kept for 8 hours.

[0046] (4) Sintering: Put the dried silicon carbide body in a silicon carbide smelting ...

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Abstract

The invention belongs to the technical field of refractory material preparation, and particularly relates to a silicon carbide ceramic product and a preparation method. Silicon carbide are used as main raw materials, the silicon carbide ceramic product utilizes introduces part of silicon carbide micro powder, adopts organic bond and introduces additives B4C (boron carbide) or elementary substanceB, and is prepared by sintering the components in an area, at the temperature of 2000-2300 DEG C, of an Acheson silicon carbide smelting furnace. The raw material components used by the silicon carbide ceramic product comprise, in mass percent, 65-75% of silicon carbide particles, 15-20% of silicon carbide fine powder and 10-15% of the silicon carbide micro powder, the additives B4C are 2-3% of the weight of the silicon carbide raw materials or the elementary substance B is 1-2% of the weight of the silicon carbide raw materials, and the bond is 3-4% of the weight of the silicon carbide raw materials. By the aid of the silicon carbide ceramic product and the preparation method, heat conductivity, high-temperature strength and chemical erosion of the product is improved.

Description

Technical field [0001] The invention belongs to the technical field of refractory material preparation, and in particular relates to a silicon carbide ceramic product and a preparation method. Background technique [0002] SiC is a synthetic raw material with two crystal structures of α and β. Among them, β-SiC is a low-temperature silicon carbide, which can exist stably below 1800°C, and will undergo a crystalline transformation above 1800°C to form α-SiC. SiC has excellent physical and chemical properties, such as high thermal conductivity, low thermal expansion coefficient, good wear resistance, stable chemical properties, etc., so it is widely used in chemical, steel, non-ferrous, abrasives and other fields. [0003] There are many types of silicon carbide products. Since the performance of the binding phase determines the performance of silicon carbide products, it can be roughly divided into three categories according to the different binding phases: 1. Silicate bonded produ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K21/02C04B35/565C04B35/622
Inventor 万龙刚王建栋刘臻李刚黄志林吴吉光
Owner SINOSTEEL LUOYANG INST OF REFRACTORIES RES