Biodiesel esterification reaction device

A technology of esterification reaction and biodiesel, which is applied in chemical/physical/physicochemical stationary reactors, biofuels, fatty acid esterification, etc., can solve the problems of small contact area, large material particle size, and slow reaction. Achieve the effects of increasing the contact area, increasing the reaction rate, and reducing the energy consumption of the reaction

Inactive Publication Date: 2012-06-20
JIANGSU HENGSHUNDA BIO ENERGY
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Problems solved by technology

[0003] One is that the ordinary push-type agitator causes the droplet size of the alcohol to be large and the specific surface area is small, resulting in a small contact area between the triglyceride and fatty acid and the alcohol, and the reaction speed is extremely slow, resulting in serious power consumption in the esterification process. Low output under the same equipment
In response to this problem, some people have changed the propulsive stirrer to other stirrers, but because the stirring intensity is small, the droplet size of the alcohol is large, the specific surface area is small, and the reaction is slow. When the stirring intensity is high, the alcohol quickly absorbs heat and vaporizes into the The alcohol recovery unit does not fully participate in the reaction in the esterification reaction unit;
[0004] The second is that the feed of alcohol is added from the top of the reaction device. Since the density of alcohol droplets is smaller than that of triglyceride and fatty acid, after the contact between alcohol and triglyceride and fatty ac

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  • Biodiesel esterification reaction device
  • Biodiesel esterification reaction device

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Embodiment Construction

[0012] Below in conjunction with accompanying drawing and specific embodiment, further illustrate the present invention, should be understood that these embodiments are only for illustrating the present invention and are not intended to limit the scope of the present invention, after having read the present invention, those skilled in the art will understand various aspects of the present invention Modifications in equivalent forms all fall within the scope defined by the appended claims of this application.

[0013] As shown in the drawings, a biodiesel esterification reaction device includes a tank body 1, an alcohol feed distributor 2, and a stirring member 3. The alcohol feed distributor 2 enters the tank body 1 from the middle and lower part of the tank body 1, and is pre-heated. The heat exchanger 4 for heating alcohol to the bubble point temperature is connected with the alcohol feed distributor 2 through a pipeline, and the alcohol is sprayed into the lower part of the ...

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Abstract

The invention discloses a biodiesel esterification reaction device, which comprises a kettle body, an alcohol feeding distributor and a stirring component, wherein the alcohol feeding distributor enters the kettle body from the middle lower part of the kettle body; and the stirring component is a hydrofoil axial flow stirring paddle. The biodiesel esterification reaction device has the advantages that: the alcohol feeding position of the biodiesel esterification reaction device and the stirring component are improved and are combined with an alcohol feeding state, so that the contact area of reaction materials is increased, an esterification reaction is undergone homogeneously, reaction time is shortened, reaction rate is raised, and reaction energy consumption is lowered; meanwhile, reactants are fully reacted, so that energy waste caused by recovery of unreacted alcohol entering from the upper part of the kettle body is reduced; and uniform stirring is performed, so that the phenomenon of carbonization in the esterification reaction caused by local overheat of the kettle body is avoided, and the temperature of a reaction system is convenient to control.

Description

technical field [0001] The invention relates to a biodiesel esterification reaction device. Background technique [0002] The reaction device of biodiesel esterification reaction adopts common propulsion type agitator, and the feed of alcohol is added dropwise in the upper part of the reaction device at the same time. This existing esterification reaction device will The following problem occurs: [0003] One is that the ordinary push-type agitator causes the droplet size of the alcohol to be large and the specific surface area is small, resulting in a small contact area between the triglyceride and fatty acid and the alcohol, and the reaction speed is extremely slow, resulting in serious power consumption in the esterification process. The output is low under the same equipment situation. In response to this problem, some people have changed the propulsive stirrer to other stirrers, but because the stirring intensity is small, the droplet size of the alcohol is large, the...

Claims

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Application Information

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IPC IPC(8): C11C3/04C11C3/10C10L1/02B01J19/18
CPCY02E50/13Y02E50/10
Inventor 陈恒顺严小建申圣良方海姣
Owner JIANGSU HENGSHUNDA BIO ENERGY
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