Polyester film for electronic tag and preparation method thereof
A technology of polyester film and electronic tags, which is applied to record carriers used in machines, instruments, computer parts, etc., can solve problems such as unstable electrical properties, poor dimensional stability, and difficult definition of reading areas, and achieve good economy Benefits and social benefits, good practical effect
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[0035] Example 1
[0036] Preparation of functional slice A: Use high-quality shell powder (commercially available) with an average particle size of less than 6μm, using titanate coupling agent (brand NDZ-201, commercially available), silane coupling agent (brand KH550, commercially available) , Surfactant (fatty acid glyceride , Commercially available) for processing, using DMT method to synthesize functional slices A with a mass percentage of 0.1-13.5% of shell micropowder under the conditions of adding polyphosphoric acid (PPA for short). Functional polyester chip A satisfies the performance indicators including: moisture 0.62dL / g, diethylene glycol ≤1.4%, and the mass percentage of shell powder 0.1~13.5%.
Example Embodiment
[0037] Example 2
[0038] Preparation of functional slice B: Put nano-montmorillonite (commercially available) into a high-speed mixer, then slowly add solvent-treated silane coupling agent (brand KH550, commercially available), and stir at high speed for 20 minutes to obtain modified nano-montmorillonite Desoil, use DMT method or PTA method to synthesize functional polyester chip B with a mass percentage of 0.5-32.6% of nano-montmorillonite. Functional slice B satisfies the performance indicators including: water content 0.62dL / g, diethylene glycol ≤1.4%, and nano-montmorillonite mass percentage 0.5~32.6%.
Example Embodiment
[0039] Example 3
[0040] Prepare recycled particles of waste polyester material. After pulverizing and heating the recycled waste polyester material without impurities, it is dehydrated, dried, removed low molecular weight, filtered, melted and extruded in a vacuum exhaust type regranulation extruder. Granulate and then dry both. The performance indicators that the recycled particles of waste polyester materials meet include: moisture content 0.59dL / g, and diethylene glycol ≤ 1.5%.
[0041] Preparation of ordinary polyester chips: the large-scale industrialized PTA method is used to synthesize ordinary polyester chips, namely basic chips, using PTA and EG.
[0042] Preparation of IPA chips: The production method is the same as that of ordinary polyester chips. IPA chips can be obtained by only replacing PTA with IPA. The mass percentage of IPA in polyester chips containing IPA is 0.2-7.8%.
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