Cloning and expression of arnox protein transmembrane 9 superfamily (tm9sf), methods and utility
A protein and DNA molecule technology used in molecular biology and biochemistry to solve problems such as linking changes in cells and tissues
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Embodiment 1
[0411] Example 1. Cloning and expression of soluble arNOX protein transmembrane 9 superfamily (TM9SF) isoform 4
[0412] The pET11b vector and BL21(DE3) competent cells were purchased from Novagen (Madison, WI). A plasmid carrying the TM9SF4 sequence was prepared by inserting the soluble TM9SF4 coding sequence into the pET11b vector (between the NheI and BamHI sites). The TM9SF4 sequence was amplified from full-length cDNA by PCR. The primers used were 5'-GATATACATATGGCTAGCATGGCGACGGCGATGGAT-3' (forward) (SEQ ID NO: 11) and 5'-TTGTTAGCAGCCGGATCCTCAGTCTATCTAGC-3' (reverse) (SEQ ID NO: 12). The PCR product was then double digested with NheI and BamHI and ligated into pET11B vector.
[0413] The DNA sequence of the ligation product (pET11b-TM9SF4) was confirmed by DNA sequencing. Then pET11b-TM9SF4 was transformed into BL21(DE3) competent cells. Single clones were picked and inoculated into 5ml LB+ampicillin (LB / AM) medium. The overnight culture (1 ml) was diluted into 100 m...
Embodiment 2
[0420] Example 2. Characterization of recombinant arNOX
[0421]The reduction of ferricytochrome c by superoxide has been adopted as a standard measure of superoxide formation (Mayo, L.A. and Curnutte, J., 1990, Meth. Enzymol. 186:567-575; Butler, J. et al. al., 1982, J. Biol. Chem. 257:10747-10750). This method is generally accepted for measuring superoxide production when used in conjunction with superoxide dismutase inhibition. The assay reagent is dissolved in PBSG buffer solution (8.06g NaCl, 0.2g KCl, 0.18g NaCl) by 150μl 2 HPO 4 , 0.13g CaCl 2 , 0.1g MgCl 2 , 1.35g of glucose dissolved in 1000ml of deionized water, adjusted to pH 7.4, filtered and stored at 4 ° C) in the buffer coating material composition. The reduction of ferricytochrome c by superoxide was monitored by the increase in absorbance at 550 nm compared to the absorbance at 540 nm (Butler et al., 1982). As another control for the specificity of arNOX activity, 60 units of superoxide dismutase (SOD) w...
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