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Corrosion inhibitor and preparation and application thereof

A technology of corrosion inhibitors and corrosion inhibitors, which is applied in the field of adding corrosion inhibitors, can solve the problems of unstable film-forming performance, poor solubility, good film-forming performance of corrosion inhibitors, etc., and achieve good dispersibility and solubility, Simple synthesis process and high corrosion inhibition efficiency

Active Publication Date: 2014-01-01
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] All of the above corrosion inhibitors can be applied to CO 2 Corrosive systems, and have good CO control 2 Corrosion effect, but there are still some deficiencies. Some corrosion inhibitors have a narrow use range and lose their protective effect with the change of corrosion system temperature; some corrosion inhibitors have unstable film-forming performance and are easy to damage defects; Corrosion inhibitors have good film-forming properties but poor water solubility and solubility; some corrosion inhibitors have a single component and cannot play a synergistic effect.

Method used

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  • Corrosion inhibitor and preparation and application thereof
  • Corrosion inhibitor and preparation and application thereof
  • Corrosion inhibitor and preparation and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 11

[0040] Embodiment 1~3 prepares component (A)

Embodiment 12

[0041] Example 1

Embodiment 1~3

[0042] Put oleic acid and diethanolamine into the reactor at a molar ratio of 1:2, raise the temperature to 140-220°C under constant stirring, and feed in N 2 Gas, reflux for 3-6 hours, reduce the reaction temperature to 70-120 °C, and add 1:2 diethanolamine, and add 0.5% NaOH, control the reaction progress with the acid value, obtain the fatty acid amide intermediate, and continue the reaction After the reaction is completed, cool the intermediate to below 50°C for 3 to 6 hours, slowly add maleic anhydride in batches according to the molar ratio of 1:1.1, and react at 70 to 110°C for 3 to 8 hours after the addition, and obtain Oleamide maleate (A) 1.

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PUM

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Abstract

The invention discloses a corrosion inhibitor and preparation and application thereof. The corrosion inhibitor consists of the following components by total weight of the corrosion inhibitor: 1 to 15 weight percent of imidazoline ester, 1 to 10 weight percent of corrosion inhibition auxiliary and 5 to 50 weight percent of solvent. At a temperature of 30 to 130 DEG C, the corrosion inhibitor has good film forming property, has excellent dispersibility and solubility property and has the corrosion inhibition rate of over 86 percent under the condition of an additive amount of 20 to 50mg / L.

Description

field of invention [0001] The invention relates to the addition of corrosion inhibitors to equipment for processing or converting hydrocarbon oils, in particular to an anti-CO 2 Corrosion inhibitors and their preparation and application. Background technique [0002] During oil and gas development, CO 2 It is often produced as associated gas at the same time, and the accompanying liquid-phase corrosive medium usually includes condensate oil in gas wells, oilfield water and its mixture. As the water cut in the oil well increases, the deep layer contains CO 2 The development of oil and gas reservoirs is increasing, CO injection 2 General promotion of enhanced oil recovery technology, CO 2 Corrosion has become an extremely prominent problem that plagues the development of the oil and gas industry and has attracted widespread attention. [0003] Humid CO 2 It will cause rapid general corrosion and severe local corrosion of steel, causing early corrosion failure of pipeline...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23F11/14
Inventor 唐应彪李朝法段永锋李春贤孙新乐刘强石运峰张庆源
Owner CHINA PETROLEUM & CHEM CORP
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