Preparation method for south China pine needle extractives and application of south China pine needle extractive in freshness of eggs
A pine needle extract and pine needle technology, applied in the field of plant extract research and application, can solve the problems of water-soluble substances in the composition, no poultry and egg preservation examples, traditional technology and methods, etc., achieve ideal extraction effect, improve antiseptic preservation , good biological effect
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Embodiment 1
[0024] A preparation method of South China pine pine needle extract and its application in the preservation of poultry eggs, the process steps are:
[0025] Pine needle collection and treatment: Choose 500g of fresh, pollution-free and disease-free pine needles of South China pine needles from middle-aged forests, rinse them with clean water in time, drain them, and pulverize them with machine-made pulp;
[0026] Freeze-thaw multiple times Put the pine needle pulp under the storage conditions of -25℃ and 4℃ and freeze-thaw repeatedly 3 times with an interval of 8 hours;
[0027] Ethanol extraction Thaw the pine needle slurry, add 2.5 liters of 45% ethanol solution, reflux in a water bath at 75°C, extract for 12 hours, and filter the filtrate;
[0028] Filtration and concentration The filter residue is extracted again for 6 hours, the filtrate is filtered and combined with the filtrate, and concentrated under reduced pressure to an extract to obtain 65 g of South China pine needles ...
Embodiment 2
[0031] A preparation method of South China pine pine needle extract and its application in the preservation of poultry eggs, the process steps are:
[0032] Pine needle collection and treatment: Select 600g of fresh, pollution-free and disease-free pine needles of South China pine needles from middle-aged forests, rinse them with clean water in time, and drain them to pulverize machine-made pulp;
[0033] Freeze-thaw multiple times Put the pine needle pulp into the storage conditions of -20℃ and 4℃ and freeze-thaw repeatedly twice, with an interval of 8 hours each time;
[0034] Ethanol extraction Thaw the pine needle pulp, add 2.5 liters of 45% ethanol solution, reflux in a water bath at 75°C, extract for 10 hours, and filter the filtrate;
[0035] Filtration and concentration The filter residue was extracted again for 6 hours, and the filtrate was filtered and combined with the filtrate, and concentrated under reduced pressure to an extract to obtain 68 g of South China pine pine...
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