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Method for preparing clean type post-processing additive for reactive dyeing cotton fabric

A reactive dye and dyed cotton technology, applied in the field of textile printing and dyeing, can solve the problems of low dyeing rate and color fixation rate, inconspicuous effect, and large color change of fabrics, so as to reduce the content of floating colors on fabrics and facilitate effective reuse , the effect of simple preparation method

Inactive Publication Date: 2012-09-19
XI'AN POLYTECHNIC UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the easy hydrolysis of reactive dyes, in the traditional process, there are problems of low dyeing rate and fixation rate
In order to ensure the color fastness, it is necessary to remove the hydrolyzed and unfixed dyes. Therefore, a post-treatment process that takes a long time, consumes a lot of energy, and consumes a lot of water is often required. In addition, the post-treatment process also brings serious pollution to the color of wastewater. And it is easy to cause disadvantages such as staining on the white background of calico
In order to solve these disadvantages, many researchers have developed some post-treatment aids and post-treatment processes to a certain extent to make up for the shortcomings of existing reactive dyes, but the existence of these post-treatment aids has certain environmental pollution (such as release of formaldehyde) , or the price is high, the effect is not obvious, or the color of the fabric treated after color fixation changes greatly, etc.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0112] Collect the chicken feathers and clean them, configure an acetic acid solution with a concentration of 0.3% by volume, pour the clean chicken feathers into the acetic acid solution at 30°C, the mass ratio of the chicken feathers to the acetic acid solution is 1:30, pre-treat for 5 minutes; use tap water Clean the chicken feathers, dry the cleaned chicken feathers at room temperature; configure 3g / L sodium bisulfite solution as a pretreatment solution, heat the pretreatment solution at a temperature of 50°C, and put the dried chicken feathers into the pretreatment solution In this method, the mass ratio of chicken feathers to the pretreatment solution is 1:10, and the pretreatment time is 10 minutes; the chicken feather protein solution is prepared according to the quality of the pretreated chicken feathers, and the mass ratio of chicken feathers to the solution is 1:10. Dissolve urea and sodium hydroxide in water to form a feather protein solution. The mass ratio of urea...

Embodiment 2

[0117] Collect the chicken feathers and clean them up, prepare a glacial acetic acid solution with a concentration of 0.5% by volume, pour the clean chicken feathers into the acetic acid solution at 40°C, the mass ratio of the chicken feathers to the acetic acid solution is 1:40, and pre-treat for 10 minutes; Wash the chicken feathers with tap water, and dry the cleaned chicken feathers at room temperature; configure 5g / L sodium bisulfite solution as a pretreatment solution, heat the pretreatment solution, and put the dried chicken feathers into the pretreatment solution at a temperature of 70°C In the solution, the mass ratio of chicken feathers to the pretreatment solution is 1:20, and the pretreatment time is 15 minutes; according to the quality of the pretreated chicken feathers, the chicken feather protein solution is prepared, and the mass ratio of the chicken feathers to the solution is 1:20, which are respectively called Dissolve urea and sodium hydroxide in water to fo...

Embodiment 3

[0122] Collect the chicken feathers and clean them up, configure an acetic acid solution with a concentration of 0.7% by volume, pour the clean chicken feathers into the acetic acid solution at 50°C, the mass ratio of the chicken feathers to the glacial acetic acid solution is 1:50, and pre-treat for 15 minutes; Wash the chicken feathers with tap water, and dry the chicken feathers after cleaning at normal temperature; configure 9g / L sodium bisulfite solution as a pretreatment solution, heat the pretreatment solution, and put the dried chicken feathers into the pretreatment solution at a temperature of 90°C. In the treatment solution, the mass ratio of chicken feathers and pretreatment solution is 1: 30, and the pretreatment time is 20min; according to the quality of chicken feathers after pretreatment, chicken feather protein solution is configured, and the mass ratio of chicken feathers and solution is 1: 30. Weigh urea and sodium hydroxide and dissolve them in water to form ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention discloses a clean type post-processing additive for a reactive dyeing cotton fabric. A method for preparing the clean type post-processing additive includes that firstly waste chicken feathers are used for preparing protein powders, then a sodium hydroxide solution is prepared, the chicken feather protein powders are dissolved with the sodium hydroxide solution, then a modifier WLS is prepared, and the chicken feather protein powders dissolved with the sodium hydroxide solution and the WLS are placed in a three-neck flask in a certain proportion and stirred at a certain temperature for some time to obtain the clean type reactive dyeing cotton fabric post-processing additive. The prepared post-processing additive has the advantages that preparing raw materials are sufficient, the price is low, biodegradation can be achieved, and the preparation is simple and convenient. According to a test, the dyed cotton fabric which is processed by the post-processing additive has the advantages that an effective color fixation can be achieved, the floating color content on the fabric is reduced, staining on white cloth is remarkably reduced during soaping, further the water consumption and the chroma pollution during floating color removing are reduced, water and energy are saved, and color fixation effect is good.

Description

technical field [0001] The invention belongs to the technical field of textile printing and dyeing, and relates to a post-processing auxiliary for fabric dyeing, in particular to a preparation method of a cleaning post-processing auxiliary for reactive dye dyed cotton fabric. Background technique [0002] At present, reactive dyes are an important class of dyes for dyeing cellulose fibers, and their applications are very extensive. However, due to the easy hydrolysis of reactive dyes, in the traditional process, there are problems of low dyeing rate and fixation rate. In order to ensure the color fastness, it is necessary to remove the hydrolyzed and unfixed dyes. Therefore, a post-treatment process that takes a long time, consumes a lot of energy, and consumes a lot of water is often required. In addition, the post-treatment process also brings serious pollution to the color of wastewater. And it is easy to cause disadvantages such as staining on the white background of ca...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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IPC IPC(8): D06P5/08D06P5/06D06P3/66
Inventor 王雪燕刘元军
Owner XI'AN POLYTECHNIC UNIVERSITY
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