Method for preparing intelligent waterproof moisture permeable tent fabric
A waterproof and moisture-permeable, tent fabric technology, applied in the field of fabric preparation, can solve problems such as insufficient trigger temperature, affecting the waterproof and moisture-permeable effect of fabrics, etc. Effect
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[0020] The preparation method of the smart waterproof and moisture-permeable tent fabric of the present invention includes the steps of preparing the shape memory polyurethane emulsion, the step of adjusting the trigger temperature of the shape memory polyurethane, the water repellent finishing step of the base fabric and the coating finishing step of the coating.
[0021] The preparation steps of shape memory polyurethane are: first add polyether polyol of different proportions into the container, then vacuumize the container and heat the polyether polyol to 110~120℃ for dehydration for 2-3h, and then lower the temperature to 65~75 After ℃, pour nitrogen into the container, then add 4,4-diphenylmethane diisocyanate MDI dissolved in N,N'-dimethylformamide DMF solution into the container, and gradually increase the temperature to 75±5℃ for reaction 1.5~2h, when the temperature is lowered to 50~60℃, gradually add N,N'-dimethylformamide DMF solution containing 1,4-butanediol BDO into...
Embodiment 1
[0027] The preparation method of the intelligent waterproof and moisture-permeable tent fabric of the present invention includes:
[0028] The preparation steps of shape memory polyurethane are: first add polyether polyol of different proportions into the container, then vacuumize the container and heat the polyether polyol to 120°C for dehydration for 2.5h, then cool to 70°C and put it in the container Blow in nitrogen, and then add 4,4-diphenylmethane diisocyanate MDI dissolved in N,N'-dimethylformamide DMF solution into the vessel, gradually increase the temperature to 75°C and react for 2h, then cool to 50°C At the time, gradually add the N,N'-dimethylformamide DMF solution containing 1,4-butanediol BDO to the container, and react at 60℃ for 1.5h, then add methanol to the container under stirring Terminate the reaction and degas in vacuum;
[0029] To adjust the trigger temperature of shape memory polyurethane, adjust the ratio of the soft and hard segments of the polyurethane...
Embodiment 2
[0034] The preparation method of the intelligent waterproof and moisture-permeable tent fabric of the present invention includes:
[0035] The preparation steps of shape memory polyurethane are the same as in Example 1;
[0036] The adjustment step of the trigger temperature of the shape memory polyurethane is to adjust the ratio of the soft and hard segments of the polyurethane through the DSC test regulator. Refer to "GB / T17594-1998 Textile Material Thermal Transition Temperature Test Method Differential Scanning Calorimetry". The temperature of the whole test is The range is -50~100℃, the heating rate is 10℃ / min, the whole test process is carried out under the protection of nitrogen, and the 4,4-diphenylmethane diisocyanate MDI, polyethylene glycol PEG, and polycarbonate in the shape memory polyurethane are adjusted. When the ratio of butylene diacid PBA and 1,4-butanediol BDO is 3.0:0.8:0.4:2.0, the trigger temperature Tg of shape memory polyurethane is 35~36℃, which can make t...
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