Composite sol for anti-reflection coating and anti-reflection coated photovoltaic glass

A composite sol, photovoltaic glass technology, applied in the direction of colloid chemistry, colloid chemistry, coating, etc., to reduce surface roughness, improve strength and weather resistance, reduce R & D and production costs

Inactive Publication Date: 2013-01-02
杭州美格玻璃有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In view of the weather resistance problems and the shortcomings of the above coating products in the use of anti-r...

Method used

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  • Composite sol for anti-reflection coating and anti-reflection coated photovoltaic glass

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] A composite sol for anti-reflection coating, prepared according to the following method from the following raw materials:

[0044] Step 1: Mix ethyl orthosilicate, ethanol, ammonia water, and water at a volume ratio of 1:10:0.2:0.15, place on a magnetic stirrer and stir at 300r / min, heat to 40°C for pre-reaction 8 Hour;

[0045] Step 2: The mixed solution in step 1 was sealed and aged for 120 hours, and sol A was obtained by back distillation to remove ammonia for 6 hours;

[0046] Step 3: Take another ethyl orthosilicate, ethanol, hydrochloric acid, and water as raw materials and mix them according to the volume ratio of 1:10:0.02:0.15. Stir and pre-react at 40°C and 300r / min for 6 hours to obtain Sol B ;

[0047] Step 4: Press sol A and sol B by SiO 2 The content is mixed evenly at a ratio of 1:0.65, sealed and aged at 40°C for 48 hours to obtain composite sol C;

[0048] Step 5: Add silane coupling agent KH-550 to composite sol C at a ratio of 0.8g / L, and stir ma...

Embodiment 2

[0054] A composite sol for anti-reflection coating, prepared according to the following method from the following raw materials:

[0055] Step 1: Mix ethyl orthosilicate, isopropanol, ammonia water and water at a volume ratio of 1:10:0.3:0.15, place on a magnetic stirrer and stir at 300r / min, heat to 40°C Reaction for 8 hours;

[0056] Step 2: Seal and age the mixed solution in Step 1 at 40° C. for 120 hours, and back-distill to remove ammonia for 6 hours to obtain Sol A;

[0057] Step 3: Take another ethyl orthosilicate, isopropanol, hydrochloric acid, and water as raw materials and mix them according to the volume ratio of 1:10:0.04:0.15, and pre-react at 40°C and 300r / min for 6 hours to obtain Sol B;

[0058] Step 4: Press sol A and sol B by SiO 2 The ratio of content 1:0.25 is mixed evenly, sealed and aged at 40°C for 48 hours to obtain composite sol C;

[0059] Step 5: Add silane coupling agent KH-550 to composite sol C at a ratio of 1.2 g / L, and hydrolyze at 40°C and...

Embodiment 3

[0065] Step 1: Mix ethyl orthosilicate, isopropanol, ammonia water and water at a volume ratio of 1:10:0.25:0.15, place on a magnetic stirrer and stir at 300r / min, heat to 40°C Reaction for 8 hours;

[0066] Step 2: Seal and age the mixed solution in Step 1 at 40°C for 120 hours, and back-distill to remove ammonia for 8 hours to obtain Sol A;

[0067] Step 3: Take another ethyl orthosilicate, isopropanol, hydrochloric acid, and water as raw materials and mix them according to the volume ratio of 1:10:0.04:0.15, and pre-react at 40°C and 300r / min for 6 hours to obtain Sol B;

[0068] Step 4: Press sol A and sol B by SiO 2 The content is mixed evenly at a ratio of 1:0.25, sealed and aged at 40°C for 48 hours to obtain composite sol C;

[0069]Step 5: Add silane coupling agent KH-570 to the composite sol C at a ratio of 1.5 g / L, and stir magnetically at 40°C and 300r / min until the hydrolysis is complete;

[0070] Step 6: Place the composite sol obtained in Step 5 for static a...

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Abstract

The invention relates to the field of manufacture of packaging glass for solar cells, and especially relates to a multi-step catalyzed composite sol for anti-reflection coating, and anti-reflection coated photovoltaic glass manufactured by the composite sol. The composite sol for anti-reflection coating is prepared from the following raw materials by the following method which comprises steps of: preparing sol A, preparing sol B, preparing composite sol C, preparing composite sol D, preparing composite sol E, and preparing the composite sol for anti-reflection coating. An anti-reflection film coated by the sol only needs coating once; therefore the production cost is low, and the process is high-efficient and easily-controlled; the composite sol of the invention is suitable for large-area coating production of photovoltaic glass; the coated product can pass related examinations, such as film hardness, adhesion, and weatherability.

Description

technical field [0001] The invention relates to the field of manufacturing packaging glass for solar cells, in particular to a multi-step catalyzed composite sol for anti-reflection coating and photovoltaic glass with anti-reflection coating manufactured by using the composite sol. Background technique [0002] In recent years, with the deterioration of the global environment and the rise of traditional energy market prices, countries around the world have introduced strategies to promote the utilization and development of new energy. Clean, safe and convenient silicon-based solar cells can not only be used on roofs and walls on a small scale to provide daily electricity for buildings, but also can be built on a large scale in areas rich in sunshine resources and connected to the grid for power generation. focus on. When the solar cell is working, the light first passes through the uppermost encapsulating glass and enters the cell component, and then is converted into elect...

Claims

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Application Information

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IPC IPC(8): C09D139/06C09D133/00C09D101/28C09D7/12B01J13/00C03C17/23
Inventor 赖博渊夏卫文王德标赵建杨董天鹏
Owner 杭州美格玻璃有限公司
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