Fuel cells, carbon composite structures and methods for manufacturing the same
A composite structure and fuel cell technology, applied in the direction of fuel cells, fuel cell parts, chemical instruments and methods, etc., can solve problems such as complicated methods, reduced battery efficiency, and increased production costs
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[0021] The invention provides a method for preparing a carbon composite structure. First, a micron oxygen web is provided. In one embodiment of the present invention, the micron oxygen fiber web may be a commercially available micron carbon fiber web such as Toray-090 or SGL-35EC after high temperature oxidation. In another embodiment of the present invention, the oxidized carbon fiber with a diameter of micron can be needle punched, paper-made or woven to form a non-woven fabric, paper-made or woven fabric, that is, a micron oxygen fiber web. In an embodiment of the present invention, the micron oxygen fiber web can be further thinned and formed, and the thinning and forming method can be thinning by hot pressing.
[0022] Next, a polymer such as polyacrylonitrile, pitch fiber or phenolic fiber is dissolved in a polar solvent to form a polymer solution. Polar solvents suitable for dissolving polymers can be N, N-dimethylformamide, N, N-dimethylethylamine, dimethyl sulfoxide...
Embodiment 1
[0031] Embodiment 1 prepares micron carbon fiber mesh
[0032] Take oxidized fibers with a diameter of 6 μm to 7 μm (oxidized fibers purchased from Xinxian (Stock) Co., Ltd.), and form a non-woven fabric with a thickness of 3 mm by needle punching. The base weight of the above non-woven fabric is 300g / m 2 . The above non-woven fabric was heated up to 1500°C at a heating rate of 10°C / min under nitrogen to carbonize the oxidized fibers of the non-woven fabric into a micron carbon fiber network. The surface resistance of the above micron carbon fiber mesh is 299mΩ / cm 2 , the volume resistivity is 7mΩ·cm, the conductivity is 133S / cm, and the pressure resistance is 100kg / cm 2 , the pore size distribution is 3-12μm.
Embodiment 2
[0033] Embodiment 2 prepares micron carbon fiber mesh
[0034] Take oxidized fibers with a diameter of 6 μm to 7 μm (oxidized fibers purchased from Xinxian (Stock) Co., Ltd.), and form a non-woven fabric with a thickness of 3 mm by needle punching. The base weight of the above non-woven fabric is 300g / m 2 . Thinning the above non-woven fabric by hot pressing to form a denser non-woven fabric with a thickness of 1.5mm. Next, the thinned non-woven fabric was placed under nitrogen, and the temperature was raised to 1500° C. at a heating rate of 10° C. / min, so that the oxidized fibers of the non-woven fabric were carbonized into micron carbon fiber nets. The surface resistance of the above micron carbon fiber mesh is 246mΩ / cm 2 , the volume resistivity is 6mΩ·cm, the conductivity is 162S / cm, and the pressure resistance is 100kg / cm 2 . Compared with Example 1, the micron carbon fiber mesh thinned by hot pressing has higher electrical conductivity.
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Abstract
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