Preparation method of light artificial soil material for green roof
A kind of artificial soil and light-weight technology, applied in the direction of botany equipment and methods, application, soilless cultivation, etc., can solve the problems of unseen literature reports and applications, and achieve light weight, ensure nutrients and porosity, and low price Effect
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Embodiment 1
[0031] 1) Preparation of acrylic acid-acrylamide composite water-absorbent resin
[0032] a. Take 3 g of NaOH and 9 mL of water to make a NaOH aqueous solution with a concentration of 7.5 mol / L, and then place it in an ice-water bath to cool to 0 °C.
[0033] b. Put a closed container in an ice-water bath, first add 7 g of acrylic acid monomer, and slowly add NaOH aqueous solution dropwise under the condition of stirring to obtain a mixed solution.
[0034] c. Then 2.8 g of acrylamide and 0.02 g of cross-linking agent N,N-dimethylenebisacrylamide were added to the mixed solution, and stirred evenly.
[0035] d. After complete dissolution, nitrogen gas was passed through the container for 10 min to remove oxygen. Then 0.03 g of initiator potassium persulfate was added, stirred vigorously, and reacted at 65 °C for 1 h, and the product was a colorless and transparent elastomer. The product is taken out, dried at a constant temperature, and pulverized to obtain an acrylic ac...
Embodiment 2
[0041] 1) Preparation of acrylic acid-acrylamide composite water-absorbent resin
[0042] a. Take 2.4 g of NaOH and 9 mL of water to make a NaOH aqueous solution with a concentration of 6 mol / L, and then place it in an ice-water bath to cool to 0 °C.
[0043] b. Put a closed container in an ice-water bath, first add 7 g of acrylic acid monomer, and slowly add NaOH aqueous solution dropwise under the condition of stirring to obtain a mixed solution.
[0044] c. Then 1 g of acrylamide and 0.0007 g of cross-linking agent N,N-dimethylenebisacrylamide were added to the mixed solution, and stirred evenly.
[0045] d. After complete dissolution, nitrogen gas was passed through the container for 10 min to remove oxygen. Then 0.007 g of initiator potassium persulfate was added, stirred vigorously, and reacted at 70 °C for 1 h, and the product was a colorless and transparent elastomer. The product is taken out, dried at a constant temperature, and pulverized to obtain an acrylic a...
Embodiment 3
[0051] 1) Preparation of acrylic acid-acrylamide composite water-absorbent resin
[0052] a. Take 1.2 g of NaOH and 9 mL of water to make a NaOH aqueous solution with a concentration of 3 mol / L, and then place it in an ice-water bath to cool to 0 °C.
[0053] b. Put a closed container in an ice-water bath, first add 7 g of acrylic acid monomer, and slowly add NaOH aqueous solution dropwise under the condition of stirring to obtain a mixed solution.
[0054] c. Then 2.1 g of acrylamide and 0.0027 g of crosslinking agent N,N-dimethylenebisacrylamide were added to the mixed solution, and stirred evenly.
[0055] d. After complete dissolution, nitrogen gas was passed through the container for 10 min to remove oxygen. Then 0.018 g of initiator potassium persulfate was added, stirred vigorously, and reacted at 70 °C for 1 h, and the product was a colorless and transparent elastomer. The product is taken out, dried at a constant temperature, and pulverized to obtain an acrylic ...
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