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Preparation method of waterless stemming used for maintaining blast furnace hearth

A technology of blister mud and blast furnace furnace, which is applied in the field of refractory materials for blast furnaces. It can solve the problems of environmental pollution, poor performance of blast furnace mud, and high production cost, and achieve the effects of good opening performance, not easy to agglomerate, and improved fluidity

Active Publication Date: 2013-09-25
临沂恒元城市建设运营有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The purpose of the present invention is to overcome the disadvantages of the prior art that the binder used for blast furnace clay is polluting the environment, and the configured clay has poor performance and high production costs, and provides a water-free foam clay for maintaining the hearth of the blast furnace The preparation method, the gun clay prepared by the present invention has good plasticity and good opening performance

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A kind of preparation method of the anhydrous foam mud that is used to maintain blast furnace hearth of the present embodiment, its specific steps are as follows:

[0029] (1) Preparation of refractory aggregate:

[0030] Weigh 13 parts of titanium dioxide, 4 parts of titanium carbide, 23 parts of corundum, 16 parts of silicon carbide, 35 parts of mullite, 6 parts of calcium-free chromium slag, 7 parts of blast furnace gas ash and 10 parts of coke according to the parts by mass. The particle size of titanium, corundum, silicon carbide, mullite and calcium-free chromium slag is required to be less than 1mm, and they are added to the mixer in sequence and mixed for 11 minutes to obtain refractory aggregate;

[0031] (2) Preparation of binder:

[0032] a) Weigh 43 parts of asphalt and 5 parts of hydrogenated terphenyl in parts by mass, add the asphalt and hydrogenated terphenyl to the reaction kettle in turn, and stir and mix at a temperature of 58°C for 18 minutes;

[0...

Embodiment 2

[0038] A kind of preparation method of the anhydrous foam mud that is used to maintain blast furnace hearth of the present embodiment, its specific steps are as follows:

[0039] (1) Preparation of refractory aggregate:

[0040]Weigh 12 parts of titanium dioxide, 5 parts of titanium carbide, 20 parts of corundum, 18 parts of silicon carbide, 30 parts of mullite, 7 parts of calcium-free chromium slag, 6 parts of blast furnace gas ash and 11 parts of coke, and add them in sequence In the mixer, mix for 10 minutes to obtain refractory aggregate;

[0041] (2) Preparation of binder:

[0042] a) Weigh 40 parts of asphalt and 6 parts of hydrogenated terphenyl in parts by mass, add the asphalt and hydrogenated terphenyl to the reaction kettle in turn, stir and mix at a temperature of 55°C for 18 minutes;

[0043] b) Weigh 10 parts of silicone resin, 11 parts of furan resin and 11 parts of melamine formaldehyde resin in parts by mass, and control the heating rate of the reactor in st...

Embodiment 3

[0048] A kind of preparation method of the anhydrous foam mud that is used to maintain blast furnace hearth of the present embodiment, its specific steps are as follows:

[0049] (1) Preparation of refractory aggregate:

[0050] Weigh 14 parts of titanium dioxide, 3 parts of titanium carbide, 25 parts of corundum, 15 parts of silicon carbide, 38 parts of mullite, 5 parts of calcium-free chromium slag, 8 parts of blast furnace gas ash and 9 parts of coke, and add them in sequence In the mixer, mix for 12 minutes to obtain refractory aggregate;

[0051] (2) Preparation of binder:

[0052] a) Weigh 50 parts of asphalt and 4 parts of hydrogenated terphenyls in parts by mass, add the asphalt and hydrogenated terphenyls to the reaction kettle in turn, and stir and mix at a temperature of 60°C for 18 minutes;

[0053] b) Weigh 12 parts of silicone resin, 8 parts of furan resin and 15 parts of melamine formaldehyde resin in parts by mass, and control the heating rate of the reactor ...

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Abstract

The invention discloses a preparation method of waterless stemming used for maintaining blast furnace hearth, belonging to the field of the refractory material used for the blast furnace. The method comprises the following steps: (1) preparation of a refractory aggregate by using the following components in parts by mass: 12-14 parts of titanium dioxide, 3-5 parts of titanium carbide, 20-25 parts of corundum, 15-18 parts of silicon carbide, 30-38 parts of mullite, 5-7 parts of calcium-free chromium residue, 6-8 parts of blast furnace gas ash and 9-11 parts of coke are weighed, added into a mixer in sequence, and then mixed for 10-12 minutes; (2) preparation of a binder; (3) the binder is added into the refractory aggregate at a mass ratio of the refractory aggregate to the binder being 100:13-15 to obtain a mixture, and the mixture is continuously mixed and stirred for 30-35 minutes to obtain a mixed substance; and (4) the mixed substance is extruded by an extruder to form a massive substance and then packaged to obtain the final product. The waterless stemming prepared by the method provided by the invention has good opening performance and moderate plasticity, is resistant to the scour corrosion of the high-temperature iron slag, can not pollute the environment, and is low in production cost.

Description

technical field [0001] The invention relates to the technical field of refractory materials for blast furnaces, in particular to a method for preparing water-free foam mud used for maintaining blast furnace hearths. Background technique [0002] Crack clay is a refractory material used to block the taphole. At present, it can be divided into two categories: water clay and anhydrous clay. Water is used as a binder. Materials used as binders are called anhydrous taphole mud. Water-filled taphole clay is used in medium and small blast furnaces with low top pressure and low degree of intensified smelting; waterless taphole clay is used in large and medium-sized blast furnaces with high top pressure and high degree of intensified smelting. The composition of blast clay can be divided into two parts: refractory aggregate and binder. Refractory aggregate refers to refractory raw materials such as corundum, mullite, and coke gems, and modified materials such as coke and mica. The...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/66C04B24/40
Inventor 高金菊
Owner 临沂恒元城市建设运营有限公司