Process for recovering copper and zinc and tin and lead by utilizing side blown converter at the bottom

A side-blown furnace and process technology, applied in zinc, tin, lead processes, and copper in tin ore fields, can solve the problems of many operations, high remelting and high smelting costs, and achieve the effect of strong adaptability

Active Publication Date: 2013-02-13
江西自立环保科技有限公司
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AI-Extracted Technical Summary

Problems solved by technology

[0002] There is no process for recovering copper, zinc, tin, and lead with slag, soot, and low-grade tin ore as raw materials; the existing technology generally enriches slag, soot, and low-grade ore through mineral processing (copper, lead, e...
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Abstract

The invention discloses a process for recovering copper, zinc, tin and lead by utilizing a side blown converter at the bottom. The process is characterized in that materials dosed and mixed from slag, ash, low-grade tin ore and flux are selected for use, the water content of the dosed and mixed materials is <= 3%, the dosed and mixed materials are stand-by, hot slag of a reduction furnace is added into a side blown converter, the dosed and mixed materials are added to the side blown converter, mixed with the hot slag of the reduction furnace for reduction smelting, the tin content of the hot slag of the reduction furnace and the dosed and mixed materials which are added into the side blown converter is more than 3%, and the silicic acid degree of the slag is 1-1.2. In the first stage, the lead and the tin are volatilized in the reduction smelting mode, and lead oxide and tin oxide are obtained through dust collection. In the second stage, vulcanizing agents are added, tin sulfide is volatilized, and tin oxide is obtained after dust collection. In the third stage the slag and the copper settles and are separated to obtain copper matte and waste slag, the slag is quenched through water, and the copper matte is cast into ingots. The process for recovering the copper, the zinc, the tin and the lead by utilizing the side blown converter at the bottom is strong in adaptability, capable of separating out valuable metal such as the copper, the lead, the zinc and the tin through one-step smelting, high in direct recovery rate, and low in valuable metal containing rate of the slag.

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  • Process for recovering copper and zinc and tin and lead by utilizing side blown converter at the bottom

Examples

  • Experimental program(1)

Example Embodiment

[0020] Example 1:
[0021] (1) Ingredients and mixing: chemical composition analysis of slag, soot and low-grade tin; mix slag, soot, low-grade tin ore and flux uniformly, and the moisture content of the material is ≤3%;
[0022] (2) Reduction smelting volatile lead, zinc, lead, zinc fume collection: first put the hot slag of the reduction furnace into the side blowing furnace, and then add the mixed materials into the side blowing furnace and the hot slag of the reduction furnace for reduction smelting. The tin content in the material after adding the hot slag of the reduction furnace and the ingredient mixture in the side blowing furnace is 10%, and the slag silicic acid degree is 1 to 1.2; the first stage reduction smelting volatile lead and zinc, and dust collection to obtain lead oxide and zinc oxide. Lead and zinc fume are collected through cloth bags, and the dust content of the fume after dust collection is ≤50mg/Nm 3; Reducing agent bituminous coal particle size in reduction smelting: less than 200 mesh particles ≥ 75%, moisture ≤ 3%, the hot slag of the reduction furnace is hoisted into the side blowing furnace by the slag bag crane;
[0023] (3) Add ferrous sulfide for smelting, sulfide volatile tin, and collect tin fume: add ferrous sulfide in the second stage, and the ferrous sulfide should be calculated based on the tin content in the furnace material. The sulfur addition is 10-20% excessive, tin sulfide Volatilize and collect dust to obtain tin oxide. Tin fume is collected through a cloth bag. After dust collection, the dust content of the flue gas is ≤50mg/Nm 3;
[0024] (4) Slag precipitation and separation of copper matte: the third stage slag and copper sedimentation and separation, to obtain matte and discarded slag, slag water quenching, matte ingot, after sedimentation and separation, the slag contains copper ≤0.2% and tin content ≤0.3%.
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