Lubricating oil base oil for hydrocarbon refrigerant and lubricating oil composition comprising same
A lubricating oil composition and lubricating oil technology, applied in the direction of lubricating compositions, base materials, organic chemistry, etc., can solve the problems of lubricating oil viscosity reduction, difficulty in reducing the amount, and poor lubricity, and achieve excellent lubricity and return Oily, stable effect
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Embodiment 1
[0033] 520 g of 2-ethylhexanol (manufactured by Kyowa Hakka Chemical Co., Ltd.) and 14.8 g of potassium hydroxide (purity: 95% by mass) as a catalyst were added to a 5 L (liter) autoclave and heated at 100°C It was treated under reduced pressure for 1 hour, and alcoholized while removing water. Next, the temperature of the autoclave was raised to 110° C., and 4176 g of propylene oxide was introduced over 10 hours. After confirming that the pressure in the autoclave was constant and that all the propylene oxide had reacted, the contents were taken out. Synthetic magnesium silicate (キヨ一ワド 600S, manufactured by Kyowa Hakka Chemical Industry Co., Ltd.) was added to the content to adsorb the catalyst, and the insoluble matter was removed by filtration. GPC measurement revealed that the obtained polyoxypropylene-2-ethylhexyl ether had a number average molecular weight (Mn) of 1170 and an impurity amount of 3% by mass. The details of the GPC measurement method will be described lat...
Embodiment 2
[0035] In addition to using 744 g of dodecanol (Calcol 2098, manufactured by Kao Corporation (Kao Corporation)) as a hydrogen divalent carbon-based alcohol, 8.4 g of potassium hydroxide was added, and after reducing pressure at 110° C. for 1 hour, 3,248 g of propylene oxide was added. Except that, polyoxypropylene lauryl ether having a number average molecular weight (Mn) of 1,000 was obtained in the same manner as in Example 1. Impurities were 2% by mass.
Embodiment 3
[0037] The number average molecular weight ( Mn) 1190 polyoxypropylene isotetradecyl ether. Impurities were 3% by mass.
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