Method for recovering silver from silver-contained waste material
A technology of waste and waste residue, which is applied in the field of silver recovery from silver-containing waste, to achieve the effects of fast reduction, high purity and cost saving
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Embodiment 1
[0032] Take 200g of spent silver catalyst with a silver content of 14wt%, add 90ml of nitric acid with a molar concentration of 3.5M, react at a temperature of 50°C for 30min, filter and wash, collect the filtrate in a 250ml three-necked reaction flask, and introduce 0.15 mol of acetylene gas; separate the precipitation of silver acetylene, slowly add 0.52mol of dimethylhydrazine to the precipitate, and stir thoroughly until the end of the reaction; simultaneously introduce the gas generated by the reaction into another solution containing silver ions, and absorb the acetylene gas generated by the reaction . After the reaction was finished, the silver powder generated by the reaction was filtered and washed, and dried to obtain 27.2 g of the silver powder.
Embodiment 2
[0034] Get 100g of spent silver catalysts with a silver content of 28wt%, add 95ml of 3.5M nitric acid, react at room temperature for 50min, filter and wash, collect the filtrate in a 250ml three-necked reaction flask, and introduce 0.52mol of acetylene gas through a flow meter; separate For silver acetylene precipitation, slowly add 0.52 mol of dimethylhydrazine to the precipitation, stir well until the reaction is over; simultaneously introduce the gas generated by the reaction into another solution containing silver ions, and absorb the acetylene gas generated by the reaction. After the reaction was finished, the silver powder generated by the reaction was filtered and washed, and dried to obtain 27.3 g of the silver powder.
Embodiment 3
[0036] Take 1000g of silver-containing waste residue (other components are mainly inert alumina) with a silver content of 1wt%, add 92.5ml of 1M dilute nitric acid and react at room temperature for 50min, filter and wash, collect the filtrate in a 250ml three-necked reaction bottle, and pass through the flow Introduce 0.05 mol of acetylene gas; separate the silver acetylene precipitate, slowly add 0.19 mol of dimethylhydrazine to the precipitate, stir well until the reaction is over; simultaneously introduce the gas generated by the reaction into another solution containing silver ions, and absorb the reaction to form of acetylene gas. After the reaction was finished, the silver powder generated by the reaction was filtered and washed, and dried to obtain 9.7 g of silver powder.
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