Method for preparing titanium plate billet

A slab and billet head technology, which is applied in the field of titanium slab preparation, can solve the problems of low production efficiency, immature titanium slab, and pressing into the surface of hot-rolled coils, and achieve small thickness tolerance, low production cost, good surface quality

Inactive Publication Date: 2013-04-03
PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When titanium slabs are produced by forging methods, it is difficult to control the thickness tolerance of the slabs, which makes it difficult to control the shape and dimensional accuracy of subsequent titanium plates or titanium coils.
At the same time, defects such as wrinkles and cracks produced during the forging process will also seriously affect the surface quality of subsequent hot-rolled coils, causing serious surface quality defects such as indentations, pits, wood grains, scratches, and heavy skins to appear on the surface of hot-rolled coils
In addition, due to the large difference in the thickness of the slab and the existence of forging defects on the surface, the amount of milling during the surface cleaning of the slab is also large, which seriously reduces the yield of the slab; in addition, the number of forging fires is high, the energy consumption is large, and the production efficiency is low, which reduces the economic benefit.
Although the die casting method can reduce the slab forging process, due to the large investment and high requirements for technical equipment, the method of producing titanium slabs by die casting is not yet mature in China and is rarely used.

Method used

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Examples

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Effect test

preparation example Construction

[0012] The present invention provides a method for preparing a titanium slab, wherein the method includes the following steps:

[0013] 1) Press the sponge titanium into an electrode block, or mix the sponge titanium and the intermediate alloy and / or metal as alloy elements to form an electrode block, weld the pressed electrode block into a cylindrical electrode, and use the cylindrical electrode Vacuum consumable arc smelting to obtain cylindrical ingots;

[0014] 2) After peeling the cylindrical ingot obtained in step 1), heat it at 800°C-850°C for 90-180 minutes, then heat it to 950°C-1050°C, hold it for 180-420 minutes, and then go through a heat forging After forging, an intermediate billet with a rectangular cross section is formed;

[0015] 3) Hot-rolling the intermediate slab obtained in step 2) to obtain a titanium slab.

[0016] According to the method of the present invention, the titanium sponge may be titanium sponge commonly used in the art. Preferably, the titanium sp...

Embodiment 1

[0030] (1) Grade 0 sponge titanium (purchased from Zunyi Titanium Industry Company, with a particle size range of 0.83-25.4mm) is pressed on a 80MN hydraulic press to form a sector-shaped electrode block with a unit weight of 126 kg; in a plasma welding box Weld into a cylindrical titanium electrode with a diameter of 835mm; then undergo secondary vacuum consumable arc melting; among them, the primary melting voltage is 36V, the melting current is 26.5KA, the stirring current is 18A, and the vacuum degree is 2Pa; the secondary melting voltage is 33V, The melting current is 32KA, the stirring current is 20A, and the vacuum is 1Pa. Melt into a cylindrical ingot with a diameter of 1000mm and a weight of 9.8 tons. After testing, the weight percentages of the components of the ingot are Fe: 0.03%, C: 0.010%, N: 0.005%, H: 0.004%, O: 0.063%, and the balance is titanium.

[0031] (2) After peeling the cylindrical ingot obtained in step (1) (the peeling thickness is 3mm), the temperatur...

Embodiment 2

[0035] (1) The first grade sponge titanium (purchased from Luoyang Shuangrui Wanji Titanium Industry Co., Ltd., with a particle size range of 0.83-25.4mm) is pressed on an 80MN hydraulic press to form a semicircular electrode block with a unit weight of 76 kg ; Welded into a cylindrical commercial pure titanium electrode with a diameter of 470mm in a plasma welding box, and then undergo secondary vacuum consumable arc melting; among them, the primary melting voltage is 36V, the melting current is 15kA, the stirring current is 8A, and the vacuum degree is 2Pa ; Secondary melting voltage is 37V, melting current is 22KA, stirring current is 8A, vacuum degree is 1Pa. Melt into a cylindrical ingot with a diameter of 660mm and a weight of 3 tons. After testing, the weight percentages of the components of the ingot are Fe: 0.043%, C: 0.015%, N: 0.004%, H: 0.007%, O: 0.067%, and the balance is titanium.

[0036] (2) After peeling the cylindrical ingot obtained in step (1) (the peeling t...

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Abstract

The invention provides a method for preparing a titanium plate billet. The method comprises the steps of pressing titanium sponge into an electrode block, or evenly mixing the titanium sponge with an intermediate alloy and/or a metal as an alloy element and then pressing for the formation of the electrode block, welding the pressed electrode block into a cylindrical electrode and smelting the cylindrical electrode by adopting vacuum consumable electro-arc for the formation of a cylindrical cast ingot; peeling the obtained cylindrical cast ingot, then performing 90-180min heat preservation at a temperature of 800 to 850 DEG C, increasing the temperature to 950 to 1050 DEG C for 180-420min heat preservation and forging the cast ingot into a rectangular intermediate billet after the forging and drawing of one heating number; and finally performing hot-rolling and cogging on the obtained intermediate billet for the formation of the titanium plate billet. With the adoption of the method for preparing the titanium plate billet, the operation is convenient and the obtained titanium plate billet is small in thickness tolerance and good in surface quality.

Description

Technical field [0001] The invention relates to a method for preparing a titanium slab. Background technique [0002] Among titanium and titanium alloy processed materials, the output of titanium plate / coil accounts for about 80% of the total processing volume. It is widely used in aviation, aerospace, weapons, petrochemical, salt, chlor-alkali, hydrometallurgy, medical, papermaking, electroplating, electrolysis, etc. Industrial field. [0003] At present, there are two methods for the production of titanium (or titanium coil) slabs in China: one is to use forging, which is mainly to first press sponge titanium or recycled scrap titanium into electrode blocks, and then assemble and weld the electrode blocks into electrode rods. The welded titanium electrode rod is smelted in a vacuum consumable arc melting furnace for 2-3 times to finally form a cylindrical titanium ingot. The titanium ingot is heated and forged through multiple fires, and finally a rectangular slab is prepared. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B23P15/00
Inventor 黄德明杨雄飞韦青峰陈永郭华
Owner PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP
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