Method of non-vacuum melting and casting copper-chromium-zirconium alloy

A non-vacuum smelting and zirconium alloy technology, which is applied in the field of non-vacuum smelting and casting copper-chromium-zirconium alloys, can solve the problems of large-scale industrial production that cannot meet the requirements, high production costs, and small production capacity. Large-scale industrial production, production cost reduction, and the effect of eliminating purchase costs

Inactive Publication Date: 2013-07-03
北京新北铜铝业有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But this method also has many disadvantages: 1. small production capacity, difficult to form large-scale production; 2. high production cost; 3. low production efficiency, difficult to produce large-scale materials; certain impact; ⑤ poor market competitiveness
Although this method can reduce oxidation burning loss, it needs a protective gas device, and self-made or purchased protective gas will increase the production cost; the addition of metal chromium in the form of a master alloy requires the preparation of a copper-chromium master alloy first, which will also increase production. cost; in addition; the gate is opened at the bottom of the induction furnace, one is that safety issues cannot be guaranteed, and the other is that it is possible to conduct a small amount of experiments as an experimental device, but it cannot meet the requirements for large-scale industrial production

Method used

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Embodiment Construction

[0022] The present invention will be further described below in conjunction with specific embodiments.

[0023] Herein, wt% all means weight percentage.

[0024] The following embodiments use a 100kw intermediate frequency induction electric furnace as the melting furnace. Copper-containing raw materials use electrolytic copper and copper-chromium-zirconium alloy smelting process return materials, and the covering agent uses a mixture of cullet and borax with a weight ratio of 1:1. Among the raw materials, the Cu content in the electrolytic copper is ≥99.95wt%, the Cr content in the metal chromium is ≥98.5wt%; the Zr content in the metal zirconium is ≥98wt%.

[0025] The following specific examples illustrate the method for non-vacuum melting and casting of the copper-chromium-zirconium alloy provided by the present invention.

[0026] (1) Bake the smelting furnace before smelting, and then put 150kg of electrolytic copper, 130kg of returned material and 2.9kg of covering agent (weig...

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Abstract

The invention relates to a method for non-vacuum melting and casting a copper-chromium-zirconium alloy. The method comprises the steps of drying an oven, loading a copper-containing raw material and a covering agent in a hearth of a melting furnace, melting the copper-containing raw material into copper water; (2) pulverizing chromium metal powder into particles with the particle size of 3-5 mm, putting the particles in a fire-resistant container, sealing the container, pressing the fire-resistant container into the copper water to make the chromium metal particles completely released into the copper water, and keeping a temperature of the hearth at 1,300-1,400 DEG C; (3) wrapping a zirconium metal by a copper foil, pressing the zirconium metal wrapped by the copper foil in the copper water rapidly, keeping the temperature of the hearth at 1,250-1,350 DEG C for 5-10 minutes, shutting down the furnace and slagging off; and (4) adjusting the temperature of the hearth to 1,200-1,300 DEG C, transferring a melt in the melting furnace into a casting ladle, and casting the melt. The method provided by the invention is simple in operation and low in cost, has small oxidation loss of the chromium metal and the zirconium metal, and can be produced in large-scale.

Description

Technical field [0001] The invention belongs to the technical field of non-ferrous metal processing and manufacturing, and specifically relates to a method for non-vacuum melting and casting of a copper-chromium-zirconium alloy. Background technique [0002] The chemical composition of the copper-chromium-zirconium alloy is 0.5% to 1.2% chromium, 0.05% to 0.25% zirconium, and the balance is copper. Copper-chromium-zirconium alloy has high strength and good electrical and thermal conductivity. Since it was invented in the United States, it has been widely used in high-strength and high-conductivity fields. It is currently the only high-strength, high-conductivity lead frame material that can meet the performance requirements of VLSI circuits. The tensile strength of copper-chromium-zirconium alloy: Rm≥600Mpa, electrical conductivity: λ≥80%I ACS, it also has a recrystallization temperature as high as 500℃. [0003] The primary problem in the industrial production of copper-chromium...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C1/02C22C9/00B22D21/00
Inventor 王新
Owner 北京新北铜铝业有限责任公司
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