Positive borehole wall stabilizer for oil and gas drilling and preparation method thereof
A wellbore stabilizer, a technology for oil and gas drilling, which is applied in the field of oil and gas drilling, and can solve the problems of inability to contain wellbore walls, plugging and preventing collapse, poor formation adaptability in long open-hole sections, and single action mechanism.
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[0032] The preparation method comprises the following steps:
[0033] In step S101, under stirring conditions, dissolving the asphalt in the dissolved oil heated to 120°C-140°C, and adding liquid protective agent, emulsifier, and solid protective agent after fully dissolving;
[0034] In step S102, after heat preservation and stirring at 100°C to 110°C for 1 hour to 1.5 hours, add inorganic acid, continue stirring, and heat preservation for 0.5 hour to 1 hour, then add inorganic salt solution;
[0035] In step S103, after the temperature is lowered to 80° C. to 90° C., the mixture is stirred and kept warm for 20 minutes to 30 minutes, the stirring is continued, and the material is discharged when the temperature drops to 60° C.
Embodiment 1
[0052] Example 1: Add 80g of 3# kerosene to a 500mL three-necked flask; heat the kerosene to 110°C, turn on the mixer, add 65g of 10# asphalt and 65g of 70# asphalt to the three-necked flask, heat up to 118°C and keep warm until the asphalt is completely After melting, cool down to 100°C; add 12g of liquid protective agent, 4g of emulsifier, and 6g of calcium oxide to the three-necked flask, and keep warm at 92°C for 30 minutes; add 10g of concentrated hydrochloric acid to the three-necked flask, and keep warm at 90°C for 40 minutes; Add 80 g of 10% calcium chloride solution into the three-necked flask, and keep the temperature for 20 minutes. Stop heating, and when the temperature in the three-neck flask drops to about 65°C, stop stirring, pour the sample into a sample bottle, and wait for evaluation.
Embodiment 2
[0053] Example 2: Add 90g of 3# kerosene to a 500mL three-necked flask; heat the kerosene to 115°C, turn on the mixer, add 60g of 5# asphalt and 60g of 40# asphalt to the three-necked flask, heat up to 124°C and keep warm until the asphalt is completely After melting, cool down to 105°C; add 14g of liquid protective agent, 6g of emulsifier, and 9g of calcium hydroxide to the three-necked flask, and keep warm at 97°C for 40 minutes; add 13g of concentrated hydrochloric acid to the three-necked flask, and keep warm at 95°C for 40 minutes ; Add 10% calcium chloride solution 70g in the there-necked flask and keep it warm for 20 minutes. Stop heating, and when the temperature in the three-neck flask drops to about 70°C, stop stirring, pour the sample into a sample bottle, and wait for evaluation.
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