Method for extracting volatile oil from agilawood seeds, and usage and application of volatile oil
A carbon dioxide and volatile oil technology, which is applied in the fields of health care and biomedicine, can solve problems such as complex processes, ecological imbalance of deep-sea sharks, and difficult control of operating processes, and achieve the effects of simple process flow, preventing the spread of cancer cells, and inhibiting the formation of cancer cells
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Embodiment 1
[0062] Take the dried agarwood seeds with a water content of ≤10%, crush them with a pulverizer to pass through a 40-mesh sieve, weigh 300g accurately and place them in an extraction kettle with 20L / h of CO 2 Extract at 40°C and 25MPa for 1.5h, then collect the yellow transparent oil with strong aroma in the first separation kettle (pressure 7MPa, temperature 50°C) and the second separation kettle (pressure 6MPa, temperature 50°C) under reduced pressure , namely 132g of volatile oil, the extraction rate is 44%, and the extraction rate of squalene is 16.72%.
Embodiment 2
[0064] Take the dried agarwood seeds with a water content of ≤10%, crush them with a pulverizer until they pass through a 30-mesh sieve, weigh 300g accurately and place them in an extraction kettle with 20L / h of CO 2 Extract at 40°C and 18MPa for 2h, and then collect the yellow transparent oil with strong fragrance under reduced pressure in the first separation kettle (pressure 6MPa, temperature 48°C) and the second separation kettle (pressure 5MPa, temperature 48°C). That is 117g of volatile oil, the extraction rate is 39%, and the extraction rate of squalene is 14.04%.
Embodiment 3
[0066] Take the dried Agarwood seeds with a water content of ≤10%, crush them with a pulverizer to pass through a 20-mesh sieve, weigh 300g accurately and place them in an extraction kettle with 20L / h of CO 2 Extracted at 40°C and 21MPa for 2.5h, then collected the yellow transparent oil with strong aroma in the first separation kettle (pressure 7MPa, temperature 45°C) and the second separation kettle (pressure 5MPa, temperature 45°C) under reduced pressure , namely 147g of volatile oil, the extraction rate is 49%, and the extraction rate of squalene is 19.11%.
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