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Metallographic test sample preparation method of aluminum-based ceramic mould core and silicon-based ceramic mould core

A technology of metallographic samples and aluminum-based ceramics, applied in the field of test parameters, can solve the problems of high brittleness of ceramic materials, and achieve the effect of avoiding uncontrollability and strong operability

Inactive Publication Date: 2013-09-18
AECC AVIATION POWER CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the general research on ceramic materials mainly focuses on their performance, composition, and preparation process, while the metallographic structure is rarely discussed. The fundamental reason is that ceramic materials are brittle and not as tough as metal materials. Can easily prepare ideal metallographic samples
However, in the process of research and development of ceramic materials, if the analysis of metallographic microstructure can be combined, it will bring immeasurable prospects for the research and development of ceramic materials.

Method used

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  • Metallographic test sample preparation method of aluminum-based ceramic mould core and silicon-based ceramic mould core
  • Metallographic test sample preparation method of aluminum-based ceramic mould core and silicon-based ceramic mould core
  • Metallographic test sample preparation method of aluminum-based ceramic mould core and silicon-based ceramic mould core

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Embodiment 1

[0021] This embodiment is a method for preparing a ceramic material into a microstructure sample. The ceramic material is an aluminum-based ceramic core for the turbine blade DZ125 of an aero-engine. The concrete process of this embodiment is:

[0022] The first step: making samples. A plurality of samples are cut from the parts to be observed of the aluminum-based ceramic core material and marked respectively to obtain a group of samples. In this embodiment, the number of samples is five.

[0023] Step 2: Determine the detection surface of the sample. The relatively flat surface of the two surfaces of each sample is taken as the detection surface of the sample.

[0024] The third step: mount the sample. Put each sample into each metallographic sample inlay mold. According to conventional method, with epoxy resin: dibutyl phthalate: ethylenediamine preparation mounting agent; Described epoxy resin: dibutyl phthalate: the mass ratio of ethylenediamine is 100:18: 10. Pou...

Embodiment 2

[0034] This embodiment is a method for preparing a ceramic material into a microstructure sample. The ceramic material is a silicon-based ceramic core for the aeroengine turbine blade DD6. The concrete process of this embodiment is:

[0035] The first step: making samples. A plurality of samples are cut from the parts to be observed of the silicon-based ceramic core material and marked respectively to obtain a group of samples. In this embodiment, the number of samples is 5

[0036] Step 2: Determine the detection surface of the sample. The relatively flat surface of the two surfaces of each sample is taken as the detection surface of the sample.

[0037]The third step: mount the sample. Put each sample into each metallographic sample inlay mold. According to conventional method, with epoxy resin: dibutyl phthalate: ethylenediamine preparation mounting agent; Described epoxy resin: dibutyl phthalate: the mass ratio of ethylenediamine is 100:18: 10. Pour the obtained mo...

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Abstract

The invention provides a metallographic test sample preparation method of an aluminum-based ceramic mould core and a silicon-based ceramic mould core. An automatic sampling machine is used for manufacturing metallographic test samples of the aluminum-based ceramic mould core and the silicon-based ceramic mould core through grinding and polishing so as to avoid the defects that the stress on the section of the test samples cannot be controlled in manual operation. Different types of metallographic abrasive paper is selected in rough grinding and fine grinding processes during sample preparation, pressure on the surface of the test samples and test sample preparation time are reasonably controlled, liquid suspended silicon in a test sample preparation process is applied, and a rotary speed value of grinding and an abrasive disc are reasonable controlled to obtain ideal sections of the metallographic test samples of the aluminum-based ceramic mould core and the silicon-based ceramic mould core. The interfaces of the metallographic test samples of the aluminum-based and silicon-based ceramic mould cores are clean and outlines of all combination phases are clear; material base bodies have no obvious stripping phenomena and have no preparation scratches; the metallographic test sample preparation method has the characteristic of simple and feasible preparation method.

Description

technical field [0001] This technology is used for the preparation of ceramic metallographic samples, specifically the test parameters provided for the preparation of aluminum-based and silicon-based ceramic core metallographic samples. Background technique [0002] In today's era of rapid technological development, ceramic materials are not just a so-called folk craft, but a science. Due to its characteristics of being almost free from acid and alkali corrosion, non-conductive, high hardness, particularly high chemical stability, high temperature resistance, aging resistance, and radiation resistance, it has attracted more and more attention in the fields of electronics, aviation, aerospace, medicine, etc. is widely used. However, the general research on ceramic materials mainly focuses on their performance, composition, and preparation process, while the metallographic structure is rarely discussed. The fundamental reason is that ceramic materials are brittle and not as t...

Claims

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Application Information

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IPC IPC(8): G01N1/28G01N1/32G01N1/36
Inventor 胡锴郭子静张爽李卫军赵勇
Owner AECC AVIATION POWER CO LTD
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