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Movable type catalyst charging device and charging method thereof

A technology of feeding device and catalyst, applied in feeding device, chemical instrument and method, chemical/physical process, etc., can solve the problems of poor applicability of flexible supplements, complicated operation links, and many supporting facilities, etc., and achieve easy disassembly. and maintenance, shorten the test cycle, reduce the effect of labor

Active Publication Date: 2013-10-16
陕西煤化工技术工程中心有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the structure of this device is relatively complicated, and all of them require program measurement and control. There are many supporting facilities, complicated operation links, high cost, and it is not easy to move. It is not suitable for flexible supplements in pilot plants and other devices.

Method used

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  • Movable type catalyst charging device and charging method thereof
  • Movable type catalyst charging device and charging method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0058] Dosing to the regenerator of a pilot plant, the dosing port elevation is 10m, the state of the regenerator: normal pressure, normal temperature, 20 kg of dosing is to be added, and the median diameter of the catalyst is 76-78μm. Dosing tanks are located on the ground. The main operation process: ① Weigh 20 kg of catalyst to be added on the weighing scale; ② Close the control ball valve 3, slightly open the main flow air outlet 12, the pressure gauge back blow outlet 14, and blow back air 0.1m each 3 / h, the opening of the valve of the venting pipeline 8 is 1 / 3, and the agent is added to the fluidized storage tank 2 through the funnel; ③Close the valve of the venting pipeline 8, and open the mainstreaming tuyere 12 to 0.8m 3 / h, loose air outlet 13 and pressure gauge reverse air outlet 14 each 0.1m 3 / h, pressurize the fluidized storage tank 2 until 0.10-0.15MPa; ④ open the control ball valve 3, and keep the loose air outlet 13 at 0.1m 3 / h, the lifting air outlet 15 i...

Embodiment 2

[0061] Dosing to the regenerator of a pilot plant, the dosing port elevation is 12m, the state of the regenerator: normal pressure, normal temperature, 120 kg of dosing is to be added, and the median diameter of the catalyst is 76-78μm. Dosing tanks are located on the ground. The main operation process: ① Weigh 40 kg of catalyst to be added on the weighing scale; ② Close the control ball valve 3, slightly open the main air (open the mainstream air outlet 12 valve), and the pressure gauge reverse blowing (open the reverse blowing outlet 14) each 0.1m 3 / h, the valve opening of the vent pipeline 8 is 1 / 3, and the agent is added to the fluidized storage tank 2 through the funnel; ③Close the valve 8 of the vent pipeline, and open the main air to 1.0m 3 / h, loose wind (realized by opening the loose air port 13) and pressure gauge back blow 0.1m each 3 / h, pressurize the fluidized storage tank 2 until 0.10-0.15MPa; ④ open the control ball valve 3, and keep the loose air at 0.1m 3 ...

Embodiment 3

[0064] After 50 hours of continuous operation of a pilot plant, the particle size of the catalyst in the reactor changed, and the conversion rate of raw materials decreased. In order to maintain the reaction index, 10 kg of regenerator was added to the pilot plant, and the median diameter of the catalyst was 36-38 μm. The elevation of the dosing port of the regenerator is 10m, the status of the regenerator: pressure 0.10MPa, 620°C, 10kg of supplement is required. Dosing tanks are located on the ground. The main operation process: ① Weigh 10 kg of catalyst to be added on the weighing scale; ② Close the control ball valve 3, slightly open the main air 12, and the pressure gauge reverse air 14, each 0.1m 3 / h, vent pipeline (valve) 8 opening degree 1 / 3, add agent to fluidized storage tank 2 through funnel; ③Close vent pipeline valve 8, open main air 12 to 0.5m 3 / h, loose 13 and pressure gauge blowback each 0.1m 3 / h, pressurize the fluidized storage tank 2 until 0.20MPa; ④ ope...

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Abstract

The invention discloses a movable type catalyst charging device and a charging method thereof. The device is simple in structure and convenient to operate, the main parts such as a fluidization tank and a lifting seat adopt a special structure, so that the movable type catalyst charging device is small in size and light in weight and can be conveniently moved. When the device is used for supplementing materials, the method is easy to master, the charging cost is low, and the efficiency is high. The device and the charging method provided by the invention are wide in practicality and have no special requirement on site space or condition of a pilot scale test or laboratory scale test, the charging device is simple in connection and convenient in disassembly, and the movable type catalyst charging device and the charging method can be used in the process of charging or supplementing a fluid catalyst in the pilot scale test or the laboratory scale test.

Description

technical field [0001] The invention belongs to the technical field of fluidized bed auxiliary equipment, and relates to a feeding device, in particular to a mobile catalyst feeding device and a feeding method thereof. Background technique [0002] Fluidized bed technology has been widely used in the development of new energy chemical industry, especially in the research and development of new coal chemical technology. Among them, powder catalyst is an important material to participate in the reaction. Various catalyst delivery equipment are widely used in the pilot test site, and the delivery equipment used to supplement catalyst consumption is generally called dosing tank. In the fluidized bed process, the microsphere catalyst flows continuously between the reactor and the regenerator under the high-speed airflow, so as to realize the continuous progress of the reaction and regeneration process. Due to the severe friction and collision between the particles and between th...

Claims

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Application Information

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IPC IPC(8): B01J4/00
Inventor 曹劲松温博王邓军王嘉瑞张亚秦米谦郝西维刘弓刘建斌张军民
Owner 陕西煤化工技术工程中心有限公司
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