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Manufacturing method for large format silicon carbide bamboo ceramic plate

A surface silicon carbide and manufacturing method technology, applied in the direction of manufacturing tools, pretreatment of molding materials, flat products, etc., can solve the problems of poor density uniformity, complicated operation process and high difficulty of wood ceramics, and achieve low preparation cost and high preparation process The effect of simple, good physical properties

Active Publication Date: 2013-12-04
ZHEJIANG FORESTRY UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, there are some disadvantages in the preparation methods of silicon carbide wood ceramics: first, silicon carbide is almost always treated by pressurizing or vacuumizing in a closed container, and the operation process is complicated and low in efficiency; second, silicon carbide wood ceramics The sintering is carried out in a vacuum sintering furnace or a sintering furnace protected by an inert gas, so that the size of the wood ceramics produced is small; at the same time, due to the sintering in a sealed condition, the operation process is complicated and the large-scale industrial production is difficult. The third is that the obtained wood ceramics have poor density uniformity and low strength, so it is difficult to popularize and apply
Therefore, the process technology of silicon carbide wood ceramics is obviously not suitable for making silicon carbide bamboo ceramics

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] A method for manufacturing a large-format silicon carbide bamboo ceramic plate, comprising the following steps:

[0021] (1) Preparation of high-strength bamboo slices: select 5-7-year-old Moso bamboo wood, cut bamboo sections with a greater bamboo stalk height of 4 m or more as raw materials, and then cut bamboo tubes between bamboo nodes of bamboo sections to make There are no bamboo joints on the bamboo tube, and then the bamboo tube is cut into pieces, and the bamboo green and bamboo yellow are removed after making bamboo slices, and finally 2-3mm thick bamboo slices with a uniform material thickness are cut from the dense bamboo flesh near the green part , to produce high-strength bamboo chips.

[0022] (2) Preparation of bamboo charcoal powder: Put the high-strength bamboo chips prepared in step (1) into a carbonization furnace for carbonization. The carbonization temperature is controlled between 400°C and 500°C, and the carbonization time is controlled between 7...

Embodiment 2

[0032] Compared with Example 1, the difference is: the parts by weight of each component in the step (3) are: 30 parts of bamboo charcoal powder, 50 parts of nano-silica sol, 15 parts of phenolic resin adhesive, 5 parts of isocyanate adhesive ;

[0033] With the large-format silicon carbide bamboo material ceramic plate that the present embodiment makes, physical property is as follows after testing:

[0034] The density is 0.95g / cm 3 , Vickers hardness is 7kg / mm 2 , the static bending strength is 75MPa, and the elastic modulus is 5000MPa.

Embodiment 3

[0036] Compared with Example 1, the difference is: the parts by weight of each component in the step (3) are: 20 parts of bamboo charcoal powder, 30 parts of nano-silica sol, 8 parts of phenolic resin adhesive, 2 parts of isocyanate adhesive ;

[0037] With the large-format silicon carbide bamboo material ceramic plate that the present embodiment makes, physical property is as follows after testing:

[0038] The density is 0.90g / cm 3 , Vickers hardness is 7.5kg / mm 2 , the static bending strength is 70MPa, and the elastic modulus is 5200MPa.

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Abstract

The invention discloses a manufacturing method for a large format silicon carbide bamboo ceramic plate. The method comprises the following steps of high strength bamboo chip preparation, bamboo powdered carbon preparation, mixed pulp preparation through blending, slab pavement, and pressing of the large format silicon carbide bamboo ceramic plate. The manufacturing method for the large format silicon carbide bamboo ceramic plate is simple in preparation process, a special device is not necessary, preparation cost is low, the ceramic plate with the size and specification of 2440mm*1220mm can be prepared, the prepared large format silicon carbide bamboo ceramic plate has good physical properties, the density of ceramic plate is not less than 0.95g / cm<3>, Vickers hardness is not less than 7kg / m<2>, static bending intensity is not less than 70MPa, and elasticity modulus is not less than 5000MPa.

Description

technical field [0001] The invention belongs to the field of bamboo composite materials, and in particular relates to a method for manufacturing a large-scale silicon carbide bamboo ceramic plate. Background technique [0002] A new type of porous carbon material made by impregnating wood or waste wood in thermosetting resin, and then roasting and carbonizing in a vacuum high-temperature furnace, called carbon wood ceramics, has become a research hotspot in recent years, but the raw materials for developing wood ceramics are all For wood, there are very few reports of bamboo. And my country's timber resources are extremely poor, but bamboo resources are very rich. Therefore, researching and developing bamboo ceramics and giving full play to the role of "replacing wood with bamboo" is of great significance for saving timber resources and alleviating the tension between supply and demand of timber. [0003] At present, the concept of wood ceramics has been extended, and sili...

Claims

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Application Information

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IPC IPC(8): B27M1/06B27N1/02B27N3/08
Inventor 杜春贵金春德鲍滨福
Owner ZHEJIANG FORESTRY UNIVERSITY
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