High-quality wheat germ oil and subcritical preparation method thereof
A technology of wheat germ oil and wheat germ, which is applied in the direction of fat oil/fat refining, fat oil/fat production, fat production, etc., can solve the problems of vitamin E active substance loss in finished oil, lower edible quality, and large reagent consumption, etc., to achieve Short production cycle, reduced impact, and high oil purity
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[0021] A subcritical preparation method of wheat germ oil, comprising the following steps,
[0022] A. Spread the fresh wheat germ in a microwave container, microwave for more than 3 minutes, and then pulverize the raw materials with a pulverizer;
[0023] B, the pulverized wheat germ powder particles are loaded into the extraction tank, and the solvent butane is added to carry out subcritical fluid extraction;
[0024] C. After extraction, wheat germ crude oil is obtained, and water and other impurities are removed by molecular distillation, and refined wheat germ oil is obtained after decolorization.
[0025] In the step A, the thickness of fresh wheat germ is 1-5cm, microwave treatment is carried out for 3-10min (preferably 3-5min) under the power of 400-800W, and the wheat germ is pulverized by a pulverizer for 5-20s;
[0026] In the step B, the subcritical fluid extraction conditions are, extraction pressure 0.2-1MPa, extraction temperature 5-85°C, extraction time 20-120...
Embodiment 1
[0032] A certain amount of fresh wheat germ was weighed and microwaved at 600W for 3 min, and then pulverized by a pulverizer for 10 s. Weigh 20Kg of processed raw materials in batches, and each batch and extractant—butane are put into the extraction kettle of the subcritical fluid extraction device at a material-to-solute mass-volume ratio (g / mL) of 1:3, and the extraction temperature is 25 ° C. , and the extraction pressure was 0.6MPa for 2 times, 35min each time, to obtain the extract. The wheat germ oil is put into molecular distillation, the distillation temperature is 210°C, the rotation speed is 120r / min, and the feed flow rate is 2mL / min for distillation, and then the refined wheat germ oil is obtained by decolorization process.
[0033] After testing, the inactivation rate of lipase activity of 600W3min microwave treatment was 60.08%, and the enzyme inactivation rate of lipoxygenase was 72.52%. Under the condition of accelerated storage at 37℃ for 30 days, the growth ...
Embodiment 2
[0035] A certain amount of fresh wheat germ was weighed and microwaved at 600W for 3 min, and then pulverized by a pulverizer for 10 s. Weigh 20Kg of processed raw materials in batches, put into the extraction kettle of the subcritical fluid extraction device with the extraction agent—butane at a 1:1 ratio of material to volume (g / mL), and the extraction temperature is 5°C. , under the condition of extraction pressure 0.4MPa, extract once for 25min each time to obtain the extract. The wheat germ oil is put into molecular distillation, the distillation temperature is 200°C, the rotation speed is 100 r / min, and the feed flow rate is 1 mL / min for distillation, and then the refined wheat germ oil is obtained by decolorization process.
[0036] After testing, the inactivation rate of lipase activity of 600W3min microwave treatment was 60.08%, and the enzyme inactivation rate of lipoxygenase was 72.52%. Under the condition of accelerated storage at 37℃ for 30 days, the growth rate o...
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