Ceramic silicone rubber and preparation method thereof
A technology for ceramicizing silicone rubber and silicone rubber, applied in the rubber field, can solve the problems of complicated and complicated laying and installation, falling off, and high equipment cost, and achieve the effects of improving the preparation reaction speed, good flexibility and elasticity, and reducing production costs.
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[0058] The ceramic silicone rubber of the present embodiment has two preparation methods, and the first preparation method includes the following steps:
[0059] ① Put 100 parts of the silicone rubber, 1-100 parts of silicon dioxide, 0-30 parts of silicone oil, 0.00001-10 parts of platinum complex and / or platinum compound, and 0-10 parts of coupling agent in the kneader Medium mixing;
[0060] ② Vacuumize the kneader, keep the vacuum at -0.1~-0.04Mpa, and keep the temperature at 100~200°C;
[0061] ③ Add 1 to 150 parts of vitrified powder into the kneader to knead the vitrified powder evenly with the kneaded silicone rubber, silicon dioxide, silicone oil, platinum complex and / or platinum compound, and coupling agent to form a dough Shaped ceramic rubber;
[0062] ④ move the lumpy ceramic rubber out of the kneader and cool it;
[0063] ⑤ Knead the cooled lump-shaped ceramic rubber on an open mill, add 0.1 to 10 parts of vulcanizing agent and knead to form ceramic rubber.
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Embodiment 1
[0084] Take 100 parts of dimethyl silicone rubber (MQ), 20 parts of silicon dioxide, 1 part of methyl silicone oil, 0.01 part of 1000ppm isopropanol solution of chloroplatinic acid, 0.1 part of KH560 coupling agent, 20 parts of aluminum oxide According to the first preparation method of the ceramic silicone rubber mentioned above, the ceramic silicone rubber is prepared. When the ceramic silicone rubber is vulcanized and molded, add 1 part of 2,5-dimethyl-2,5-bis(tert-butyl peroxide) oxy)hexane.
Embodiment 2
[0086] Take 100 parts of methyl vinyl silicone rubber (VMQ), 100 parts of silicon dioxide, 30 parts of hydroxyl silicone oil, 10 parts of 1000ppm isopropanol solution of chloroplatinic acid, 0.1 part of A171 coupling agent, 150 parts of silicon dioxide According to the first preparation method of ceramic silicone rubber mentioned above, ceramic silicone rubber is prepared. When ceramic silicone rubber is vulcanized and molded, 2 parts of 2,4-dichlorobenzoyl peroxide (commonly known as double-two-four) are added. .
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