Anti-yellowing energy-saving lamp adhesive and preparation method thereof
A technology of energy-saving lamps and adhesives, applied in the direction of monocarboxylic acid ester copolymer adhesives, adhesive types, non-polymer adhesive additives, etc., can solve the problem of easy yellowing of the adhesive layer, heat resistance and The problem of poor UV resistance, affecting the appearance and service life of energy-saving lamps, etc., achieves the effect of improving yellowing resistance and simple operation.
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Embodiment 1
[0020] The anti-yellowing energy-saving lamp adhesive of the present invention is carried out according to the following steps: 300 grams of milky white glue is placed in a 500 ml glass beaker, the stirring device is started to stir for 10 minutes, and then slowly added 30 grams of talcum powder and 170 gram of precipitated silica, and stir evenly; then add 2.5 grams of 2-hydroxy-4-n-octyloxybenzophenone (UV-531), 1.25 grams of 2,2'-methylenebis(4-methyl-6 tert-butylphenol) (antioxidant 2246) and 1.5 g of N,N′-diacetyl adipate dihydrazide dissolved in 20 ml of industrial ethanol, and kept stirring for 60 minutes to obtain a white viscous paste. The energy-saving lamp adhesive of the present invention is obtained.
Embodiment 2
[0022] The yellowing-resistant energy-saving lamp adhesive of the present invention is carried out according to the following steps: 270 grams of milky white glue is placed in a 500-ml glass beaker, and the stirring device is started to stir for 8 minutes, and then, under stirring, slowly add 42 grams of talcum powder and 168 gram of precipitated silica, stir evenly; then add 1.5 grams of 2-hydroxy-4-n-octyloxybenzophenone (UV-531), 1 gram of 2,6-di-tert-butyl-4-methylphenol (Antioxidant 264) and a solution formed by dissolving 0.75 g of N,N'-diacetyl adipic acid dihydrazide in 20 ml of industrial ethanol, and stirring continuously for 50 minutes to obtain a white viscous paste, which is the present invention Adhesive for energy-saving lamps.
Embodiment 3
[0024] The anti-yellowing energy-saving lamp adhesive of the present invention is carried out according to the following steps: 330 grams of milky white glue is placed in a 500-ml glass beaker, the stirring device is started to stir for 15 minutes, and then under stirring, slowly add 38 grams of talcum powder and 152 gram of precipitated silica, stir evenly; then add 5 grams of 2-hydroxy-4-n-octyloxybenzophenone (UV-531), 2 grams of tetrakis[3-(3ˊ,5-di-tert-butyl- 4'-hydroxyphenyl) propionate] pentaerythritol ester (antioxidant 1010) and 1 g of 2,2-oxalamido-bis[ethyl-3-(3,5-di-tert-butyl-4-hydroxyphenyl) )] Propionate is dissolved in 20 milliliters of industrial ethanol to form a solution, and the stirring is continued for 65 minutes to obtain a white viscous paste, and the energy-saving lamp adhesive of the present invention is obtained.
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