Antibacterial cortex phellodendri-nanosilver superfine glass fiber air filtering material
A technology of ultra-fine glass fiber and air filter material, applied in the fields of filtration and separation, deodorization, chemical instruments and methods, etc., can solve the problems of easy mass reproduction environment, secondary pollution, easy blocking, etc., and achieve high safety and efficacy. Long-lasting, pronounced bacteriostatic effect
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[0017] The preparation steps of described Phellodendron Phellodendri extract are as follows: take 15 grams of Chinese medicine Phellodendron Phellodendri decoction pieces, add 300ml of water, boil, concentrate and filter to obtain 150ml of concentrated filtrate, air-dry at 80°C and leave to stand to obtain solid Phellodendron Phellodendri precipitation, after drying, prepare into fine powder particles;
[0018] The preparation step of described silver elemental nanoparticle is as follows: get 22.8 g tetradecanoic acid and be dissolved in 140 mL methanol and the water that mix by 2:5 ratio, add the sodium hydroxide of 4g to precipitate in solution, filter, precipitate Adding to 100 mL concentration is 10 mol / L water-soluble silver nitrate solution to obtain silver myristate; Weigh 27.8ml concentration and be 20 mmol / L silver myristate in 100 mL beaker, add 58 Triethylamine with a concentration of 40 mmoL / L was stirred electromagnetically at 80°C for 2 hours, the white silver my...
Embodiment 1
[0024] 1. Preparation of Phellodendron Phellodendri Extract: Get 600 grams of Chinese medicine Phellodendron Phellodendri decoction pieces, add 12000ml of water, boil, concentrate and filter to obtain 6000ml of filtrate after concentration, air-dry and leave standstill under 80°C to obtain solid Phellodendron Phellodendri precipitation, and make fine powder after drying 300 grams of powder granules.
[0025] 2. Preparation of water-soluble silver nanoparticles:
[0026]2. Dissolve 22.8 g of myristic acid in 140 mL of methanol and water mixed at a ratio of 2:5, add 4 g of sodium hydroxide to the solution to precipitate a precipitate, filter, and add the precipitate to 100 mL with a concentration of 10 mol / L Obtain silver myristate in water-soluble silver nitrate solution; Weigh 27.8ml concentration and be 20mmoL / L silver myristate in the 100mL beaker, add 58mL concentration in the beaker and be the triethyl ether of 40mmoL / L Amine, electromagnetically stirred at 80°C for 2 hou...
Embodiment 2
[0029] 1. Preparation of Phellodendron Phellodendri Extract: Get 600 grams of Chinese medicine Phellodendron Phellodendri decoction pieces, add 12000ml of water, boil, concentrate and filter to obtain 6000ml of filtrate after concentration, air-dry and leave standstill under 80°C to obtain solid Phellodendron Phellodendri precipitation, and make fine powder after drying 300 grams of powder granules.
[0030] 2. Preparation of water-soluble silver nanoparticles:
[0031] 2. Dissolve 22.8 g of myristic acid in 140 mL of methanol and water mixed at a ratio of 2:5, add 4 g of sodium hydroxide to the solution to precipitate a precipitate, filter, and add the precipitate to 100 mL with a concentration of 10 mol / L Silver myristate is obtained in a water-soluble silver nitrate solution; 73.4ml of silver myristate with a concentration of 20 mmoL / L is weighed in a 100 mL beaker, and 58 mL of triethyl ether with a concentration of 40 mmoL / L is added to the beaker. Amine, electromagnetic...
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