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Chemical drying water removal method

A drying and chemical technology, applied in the direction of drying solid materials, drying solid materials without heating, drying, etc., can solve problems such as battery performance impact and hazards, achieve breakthroughs in production bottlenecks, remove moisture, and improve drying effects

Active Publication Date: 2014-06-04
VIGOR GAS PURIFICATION TECHNOLOGIES (SUZHOU) CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, if you do not enter the liquid injection workshop immediately, the water content will become higher due to the absorption of moisture in the air, which is far from the requirement that the water content of the lithium battery electrolyte is less than 30ppm, which will greatly affect the performance of the battery.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Example 1, taking the application of battery core drying in the lithium battery industry as an example

[0020] In the container with battery cores, inject trimethyl indium equivalent to at least 1 times the total water content of all battery cores through an accurate sampling system, trimethyl indium volatilizes, and quickly mixes with the surface of the dried battery cores and the gaps Water molecules react, the reaction principle is that trimethyl indium reacts with water to generate methane gas, indium oxide or indium hydroxide and transition products.

[0021] After passing through the desiccant trimethylindium, let it stand for a period of time until the trimethylindium reacts completely with the water in the dried battery core.

[0022] Then evacuate for 10 minutes, or purge with dry high-purity inert gas to remove excess substances and by-products.

[0023] According to the Karl Fischer coulometer test, the water content of the battery cells dried by this metho...

Embodiment 2

[0024] Example 2, taking the application of transformer insulation fiber drying in the electrical industry as an example

[0025] In the container with battery cores, inject trimethylaluminum equivalent to at least 1 times the total water content of all insulating fibers through an accurate sampling system, trimethylaluminum volatilizes, and quickly mixes with the surface and gaps of the dried insulating fibers Water molecule reaction, the reaction principle is that trimethylaluminum reacts with water to generate methane gas, aluminum oxide or aluminum hydroxide and transition products.

[0026] After passing through the desiccant trimethylaluminum, let it stand for a period of time until the trimethylaluminum reacts completely with the water of the dried insulating fiber. Then vacuumize for more than 20 minutes, or purge with dry high-purity inert gas to remove excess substances and by-products.

[0027] According to the Karl Fischer coulometer test, the moisture content of ...

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PUM

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Abstract

The invention provides a chemical drying water removal method. The method comprises the steps of firstly, putting matter which is used as a drying agent and has a high reaction with water into a container containing a dried object, secondly, vacuumizing the container, or putting dry high-purity inert gas into the container, or vacuumizing the container, and then putting the drying gas into the container for blowing, and removing residual drying agents and by-reactant. According to the method, the drying effect on solid materials is greatly improved, the effect of better removing the water is obtained, drying can be more thoroughly carried out, the higher requirement of some industries for the drying effect can be met, and especially, the production bottleneck, generated by the quite high water requirement, of industries, like a lithium-ion electric industry, can be broken through.

Description

technical field [0001] The invention relates to the field of drying, in particular to a method for chemical drying and water removal of solid materials. Background technique [0002] At present, in the field of drying, the drying of solids is mostly carried out by heating, decompression and freezing. The more common methods are ovens, vacuum ovens, etc., among which vacuum ovens have better drying effects. The application process of the vacuum oven is to place the dry material in a closed drying room, and heat the material to be dried while vacuuming with a vacuum system, so that the moisture inside the material diffuses to the surface through the pressure difference or concentration difference, and the water molecules in the material The surface obtains sufficient kinetic energy, and after overcoming the mutual attraction between molecules, it escapes to the low-pressure space of the vacuum chamber, and is thus sucked away by the vacuum system. During the vacuum drying pro...

Claims

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Application Information

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IPC IPC(8): F26B5/16F26B5/04
Inventor 张德龙
Owner VIGOR GAS PURIFICATION TECHNOLOGIES (SUZHOU) CO LTD
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