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An electrolytic cell and electrochemical technology, applied in the field of electrolytic cells, can solve the problems of poor accuracy, reduce the current transmission efficiency of the electrolytic cell, increase the distance between the working electrode and the counter electrode, etc., achieve compact structure, realize portability, improve The effect of space utilization
Active Publication Date: 2014-09-10
HANGZHOU GREAN WATER SCI & TECH INC
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[0004] However, in the electrochemical electrolytic cell with stirring function provided by the prior art, the electroplated mercury film or bismuth film on the working electrode will fall off when stirring; and the working electrode is built in the stirring rod, increasin
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Embodiment 1
[0066] The electrochemical electrolytic cell that the embodiment of the present invention 1 provides is as figure 1 shown, including:
[0067] A base 10 with a groove; a cuvette 12 arranged in the groove of the base 10; a transparent shell 13 arranged around the cuvette 12; a fixed support structure 18; Working electrode 8, reference electrode 14 and counter electrode 20; motor 19 fixed on the fixed support structure 10, upper magnet 2 connected to the motor 19; lower magnet 5 arranged below the upper magnet 2; The stirring paddle 9 connected to the lower end magnet 5, the working electrode 8, the reference electrode 14 and the counter electrode 20 are distributed around the stirring paddle 9; the bearing 7 arranged on the outside of the stirring paddle 9; bonded to the The heating rod 11 inside the stirring paddle 9, the heating rod 11 is connected to the first conductor 16 by an electric wire, the tip of the first conductor 16 is in contact with the second conductor 4, and ...
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Abstract
The invention provides an electrochemical electrolytic cell which comprises a solution containing device, a working electrode and a reference electrode which are arranged in the solution containing device, a stirring device in the solution containing device, and a heating device in the stirring device, wherein the working electrode and the reference electrode are distributed on two sides of the stirring device. According to the electrochemical electrolytic cell provided by the invention, the heating device is arranged in the stirring device, so that the electrochemical electrolytic cell can simultaneously achieve stirring and heating functions, and has stable electrochemical reaction conditions in the working process. Therefore, the electrochemical electrolytic cell provided by the invention is high in accuracy in the process of detecting heavy metal ions.
Description
technical field [0001] The invention relates to the technical field of electrolytic cells, in particular to an electrochemical electrolytic cell. Background technique [0002] Heavy metals mainly refer to metals or metalloids such as mercury, cadmium, lead, chromium, arsenic, etc., and also refer to general metals with certain toxicity, such as copper, zinc, nickel, cobalt, tin, etc. Heavy metals are enriched in the surrounding environment of human beings, enter the human body through the atmosphere, water, food, etc., and accumulate in some organs of the human body, causing chronic poisoning and endangering human health. Therefore, the detection of heavy metals has become the focus of attention. At present, heavy metal detection methods mainly include atomic absorption spectrometry, ultraviolet-visible spectrophotometry, atomic fluorescence method, electrochemical method, X-ray fluorescence spectrometry, etc. Among them, electrochemical method is a kind of heavy metal dete...
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