Preparation method of acid-modified caustic calcined magnesia/bentonite water treatment chemicals

A technology of bentonite and lightly burned magnesium, which is applied in the direction of flocculation/sedimentation water/sewage treatment, etc., to achieve the effect of abundant stock, good removal effect and simple preparation process

Inactive Publication Date: 2014-11-12
SHENYANG INSTITUTE OF CHEMICAL TECHNOLOGY
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  • Abstract
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is to provide a method for preparing acid-modified light-burned magnesite / bentonite water treatment agent. The materials of this method are derived from natural low-grade magnesite and calcium-based bentonite, which have abundant stock and low cost, and solve the problem of low-grade magnesite The comprehensive utilization of ore and bentonite provides a way out for its rational development and utilization, and enriches the varieties of water treatment agents

Method used

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  • Preparation method of acid-modified caustic calcined magnesia/bentonite water treatment chemicals

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Embodiment Construction

[0016] Below in conjunction with embodiment, the present invention is described in further detail.

[0017] Add 200g of lightly burned magnesium powder (65% MgO content) and 100g of calcium-based bentonite into a 500mL large beaker, slowly add 360mL of industrial hydrochloric acid with a mass fraction of 9%, stir while adding, heat to 450C in a water bath, and continue to stir and mix for 30 minutes After static activation for 30 minutes, heat and dry to constant weight, take it out and cool it, and grind it into powder, which is the prepared light-burned magnesium / bentonite water treatment agent product. This product is used to treat five kinds of reactive dyes and mixed dyes simulated wastewater commonly used in printing and dyeing factories, and all of them have received good treatment effects under alkaline conditions. The processing results are shown in Table 1.

[0018] Table 1 water treatment agent decolorization effect on various dye wastewater

[0019]

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Abstract

The invention provides a preparation method of acid-modified caustic calcined magnesia/bentonite water treatment chemicals and belongs to water treatment chemical preparation methods. The method comprises the steps that a certain amount of caustic calcined magnesia and a certain amount of bentonite are weighed according to the mass ratio of 1.5-2:1 (g/g); technical hydrochloric acid with the mass fraction of 9% is added into the caustic calcined magnesia and the bentonite according to the mass-to-volume ratio of 1:1.2 (g/mL); the mixture is stirred, mixed and acidized for 30 minutes at the temperature ranging from 45 DEG C to 55 DEG C and then subjected to standing for 30 minutes; after being subjected to microwave irradiation or high-temperature drying, the obtained product is smashed, and then the prepared acid-modified caustic calcined magnesia/bentonite water treatment chemicals are obtained. According to the preparation method, production raw materials comprise low-grade caustic calcined magnesia powder, the calcium bentonite and the low-concentration technical hydrochloric acid; the preparation process is simple, no waste water and waste residues are generated, and the acid-modified caustic calcined magnesia/bentonite water treatment chemicals are low in production cost and friendly to environment, are novel water treatment chemicals integrating the functions of coagulation, adsorption, filtration and the like, have a wide pH application range to reactive dyes, heavy metal and other pollutants and have a good effect on removing the reactive dyes, the heavy metal and other pollutants.

Description

technical field [0001] The invention relates to a preparation method of a water treatment agent, in particular to a preparation method of an acid-modified light-burned magnesium / bentonite water treatment agent. Background technique [0002] Water treatment agents (coagulants) include inorganic coagulants and organic polymer coagulants. Inorganic coagulants are mostly iron salts, aluminum salts, magnesium salts and inorganic polymer coagulants. Due to the complex manufacturing process, serious environmental pollution, high price of some products, certain toxicity, easy to cause secondary pollution and other reasons for the above-mentioned water treatment agents, as well as the existence of many types of industrial wastewater, great changes in water quality, and difficult to handle, etc., Its production and use are subject to certain restrictions and influences. Therefore, the development of water treatment agents is forced to gradually move towards the direction of "polyme...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F1/52
Inventor 刘桂萍刘学贵刘长风宁志高
Owner SHENYANG INSTITUTE OF CHEMICAL TECHNOLOGY
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