Method for detecting content of sulfite in wine by using ozone oxidation luminescence spectrum
A technology of sulfite and ozone oxidation, which is applied in the measurement of color/spectral characteristics, etc., can solve the problems of the influence of detection results, large consumption of reagents, long detection cycle, etc., and achieve the effect of improving wine quality and fast detection speed.
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Embodiment 1
[0058] A method for detecting sulfite content in wine using ozone oxidation luminescence spectroscopy, the working principle of the method is as follows:
[0059](1), use the detection instrument to detect a variety of (such as n types) different wines, obtain the ozonation luminescence spectra of n types of wines, take the average value of these spectra, and obtain the average ozonation luminescence spectra of the wines (see image 3 , the abscissa in the figure represents the wavelength of the spectrum, the unit is nm, the ordinate represents the number of photons, the unit is one, the same below), the wavelength λ1=490nm at the peak Gmax of the average spectral photon number is taken as the characteristic wavelength, and the characteristic wavelength λ1 corresponds to The peak photon number Gmax=84.05 is used as the weighted base for backup;
[0060] (2) Use the national standard GB / T15038-2006 method to detect the sulfite content of the above n different wines, and obtain ...
Embodiment 2
[0069] Embodiment 2 compares the spectra of sulfite solution and tested wine sample, and the steps are as follows:
[0070] (1), use the ozone generator 17 to generate ozone gas, the concentration range of ozone is 20mg / L, control the ozone peristaltic pump 14 so that the flow rate is 100mL / min, and send the ozone gas into the reaction chamber 3;
[0071] (2) Use the sample peristaltic pump 2 to send the wine sample into the reaction chamber 3 with a flow rate of 80mL / min;
[0072] (3) After the ozone gas passes through the microporous gas-permeable membrane 15, it mixes with the wine sample in the reaction chamber of the reaction chamber, and continuously and evenly contacts with the wine sample for chemical reaction to produce chemiluminescence;
[0073] (4), the condenser mirror system 4 receives the luminous signal, the condenser mirror system 4 converges the light energy to the collimator mirror 5, and the collimator mirror 5 converges to the receiving port of the optical...
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