Water-based curtain casting slurry for NFC (near field communication) magnetic substrate, preparation method of slurry and NFC magnetic substrate
A water-based, casting slurry technology for substrates, applied in the field of near-field communication, can solve the problems of difficult slurry degassing, harsh production conditions, long drying time, etc., achieve easy defoaming of slurry, reduce production costs, Reduce the effect of the pressing process
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Embodiment 1
[0030] Embodiment 1: An NFC magnetic substrate prepared by the following method:
[0031] S1. Raw material preparation: Weigh each raw material according to the following ratio and set aside; nano-scale ferrite powder (particle size: 300-500nm): 40kg; polyacrylic acid: 0.1kg; polyvinyl alcohol: 0.5kg; polyethylene glycol : 0.3kg; polyether defoamer: 0.3kg; water: 8kg;
[0032] S2. Prepare casting slurry: Mix the nano-scale ferrite powder, polyacrylic acid, polyvinyl alcohol, polyethylene glycol, and water weighed in step S1, and then ball mill for 20 hours. The ball milling speed is 300r / min. Obtain cast slurry;
[0033] S3. Defoaming stale: Pass the casting slurry prepared in step S2 through a 100-mesh sieve, add polyether defoamer, and perform vacuum defoaming for 8 hours under a negative pressure environment of 0.1MPa, and perform stale treatment at 1h / L , control the viscosity at 10000cps, and prepare the NFC magnetic substrate water-based casting slurry;
[0034] S4. T...
Embodiment 2
[0036] Embodiment 2: An NFC magnetic substrate prepared by the following method:
[0037] S1. Raw material preparation: Weigh each raw material according to the following ratio and set aside; nano-scale ferrite powder (particle size: 300-500nm): 81kg; polyacrylic acid: 0.5kg; polyvinyl alcohol: 1.5kg; polyethylene glycol : 1.0kg; polyether defoamer: 1.0kg; water: 15kg;
[0038] S2. Prepare casting slurry: mix the nano-scale ferrite powder, polyacrylic acid, polyvinyl alcohol, polyethylene glycol, and water weighed in step S1, and then ball mill for 30 hours. The ball milling speed is 500r / min. Obtain cast slurry;
[0039] S3. Defoaming stale: Pass the casting slurry prepared in step S2 through a 200-mesh sieve, add polyether defoamer, perform vacuum defoaming for 15 hours under a negative pressure environment of 0.3MPa, and perform stale treatment at 2h / L , the viscosity is controlled at 15000cps, and the NFC magnetic substrate water-based casting slurry is prepared;
[0040]...
Embodiment 3
[0042] Embodiment 3: An NFC magnetic substrate prepared by the following method:
[0043] S1. Raw material preparation: Weigh each raw material according to the following proportions and set aside; nano-scale ferrite powder (particle size: 300-500nm): 55kg; polyacrylic acid: 0.2kg; polyvinyl alcohol: 1kg; polyethylene glycol: 0.5kg; polyether defoamer: 0.5kg; water: 10kg;
[0044] S2. Prepare casting slurry: Mix the nano-scale ferrite powder, polyacrylic acid, polyvinyl alcohol, polyethylene glycol, and water weighed in step S1, and then ball mill for 24 hours. The ball milling speed is 365r / min. Obtain cast slurry;
[0045] S3. Defoaming and aging: Pass the casting slurry prepared in step S2 through a 130-mesh sieve, add polyether defoaming agent, and perform vacuum defoaming for 10 hours under a negative pressure environment of 0.2MPa, and perform aging at 1.4h / L Treatment, control the viscosity at 12000cps, and make the NFC magnetic substrate water-based casting slurry; ...
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