Treatment method for acid pickling water and neutralized waste water in tetrabromobisphenol A producing process
A tetrabromobisphenol and treatment method technology, applied in water/sewage multi-stage treatment, water/sludge/sewage treatment, chemical instruments and methods, etc., can solve the problems of limitation, incomplete oxidation, easy carbon deposition, etc. Achieve the effects of improving water production efficiency, realizing salt recycling, and reducing toxicity
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[0031] Example 1: Neutralization wastewater treatment
[0032] The pH of the neutralized wastewater was adjusted to 1.5 with sulfuric acid to generate tribromophenol precipitation. After adding polyacrylamide flocculant, the tribromophenol was separated by a centrifuge. The separated clear liquid was heated to 60°C and flashed at -0.09MPa Evaporate and flash out 10% condensate, and the residual liquid will be steam heated to concentrate and crystallize, and the crystalline solid is recovered.
[0033] According to the above experimental parameters, the experimental conditions are shown in Table 2.
[0034] Table 2: Water quality of neutralization wastewater treatment
[0035]
[0036] From the experimental results in Table 2, it can be seen that the concentration of chlorobenzene in the flashed 10% condensate is 436.4~510.4mg / L, the salinity is 0, and the 10% condensate can be recycled; the concentration of chlorobenzene in the condensate is 0 ~0.8mg / L, the salinity is 0, the condens...
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[0037] Example 2: Treatment of pickling wastewater
[0038] The pickling wastewater directly enters the flash evaporation device, flashes at 80°C and -0.09MPa, flashes 10% condensate, the residual liquid vapor is heated to concentrate and crystallize, and the crystalline solid is recovered. According to the above experimental parameters, the experimental conditions are shown in Table 3.
[0039] Table 3: Water quality of pickling wastewater treatment
[0040]
[0041] From the experimental results in Table 3, it can be seen that the concentration of chlorobenzene in the flashed 10% condensate is 37.16-105.5mg / L, the salinity is 0, and the 10% condensate is recycled; the concentration of chlorobenzene in the condensate is 0.34~ 0.48mg / L, the salinity is 0.05~0.13mg / L,
[0042] The condensate can also be recycled.
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