Method for carrying out isosynthesis on geraniol by adopting linalool
A technology of isomerization synthesis and linalool, applied in the direction of isomerization preparation, chemical instruments and methods, preparation of organic compounds, etc., can solve the problems of large amount of auxiliary materials, complicated process, difficult reaction, etc., and achieve consumption of auxiliary materials Less, simple process route, easy to control the effect of the reaction
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Embodiment 1
[0014] The method for the synthetic geraniol of this linalool isomerization is:
[0015] Add 0.8kg of linalool, 0.6kg of cinnamyl acetate, 0.002kg of dibutyltin dilaurate and 0.004kg of ammonium vanadium oxide into the reaction kettle, raise the temperature to 170°C, stir for 8 hours, then undergo hydrolysis and rectification under reduced pressure, Discharge.
[0016] The total alcohol content of the geraniol obtained in the present embodiment is 98%.
Embodiment 2
[0018] The method for the synthetic geraniol of this linalool isomerization is:
[0019] Add 0.9kg of linalool, 0.7kg of cinnamyl acetate, 0.003kg of stannous octoate and 0.007kg of vanadium pentoxide into the reaction kettle, raise the temperature to 180°C, stir for 10 hours, then undergo hydrolysis, rectification under reduced pressure, and discharge .
[0020] The total alcohol content of the geraniol obtained in the present embodiment was 98.5%.
Embodiment 3
[0022] Add 1kg of linalool, 0.8kg of cinnamyl acetate, 0.004kg of dibutyltin diacetate and 0.01kg of ammonium vanadium oxide into the reaction kettle, raise the temperature to 190°C, stir for 12 hours, then undergo hydrolysis, rectification under reduced pressure, and discharge.
[0023] The total alcohol content of the geraniol obtained in the present embodiment is 99%.
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