Tea leaf-polyolefin composite material and preparation method thereof
A composite material and polyolefin technology, applied in the field of chemistry, can solve the problems of high cost of biodegradable materials, unfavorable long-term production and use, difficult to promote and use on a large scale, and achieve strong functional advantages, strong cost advantages, and low prices. Effect
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Embodiment 1),( Embodiment 2)
[0033] The chemical name of the antioxidant 1010 used in the embodiment of the present invention is tetrakis[methyl-β-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate] pentaerythritol ester, which is produced by Shijiazhuang Yima Chemical Industry Co., Ltd. Co., Ltd. (Example 1), Zibo Xiangdong Chemical Co., Ltd. (Example 2), Shijiazhuang Baina Chemical Auxiliary Co., Ltd. (Example 3), Hangzhou Shangyou Chemical Co., Ltd. (Example 4) ), produced by Zhengzhou Haichuan Chemical Co., Ltd. (Example 5).
[0034] The model of the co-rotating parallel twin-screw extruder used in the embodiment of the present invention is TSE-65B, a product of Nanjing Hisilicon Extrusion Equipment Co., Ltd., and the working parameters are: main engine power 75kw, vacuum negative pressure -0.08~-0.05Mpa.
[0035] The screw diameter of the co-rotating parallel twin-screw extruder used in the embodiment of the present invention is 71 mm, and the aspect ratio is 44.
[0036] The high-speed mixer model that...
Embodiment 1
[0040] A tea polyolefin composite material of the present invention is made of the following raw materials in mass percentage: 30% of tea fine powder treated with silane coupling agent, 58% of polyethylene, 10% of maleic anhydride grafted polyethylene, 0.5% of stearic acid %, PE wax 1%, antioxidant 0.5%.
[0041] A preparation method of tea polyolefin composite material, comprising the following steps:
[0042] Step 1: Process the tea leaves into 150-mesh fine powder with a mechanical mill; immerse the fine powder in a diluted solution of KH550 silane coupling agent with a weight concentration of 3.0%, and soak for 4 hours under stirring; filter and separate the soaked fine powder Solid, dried at 82°C for 40 hours to obtain agglomerate powder; then use a mechanical mill to break up the agglomerate powder, and then dry at 82°C to constant weight to obtain tea fine powder treated with silane coupling agent ;
[0043] Step 2, prepare tea fine powder, polyethylene, maleic anhydr...
Embodiment 2
[0050] A tea polyolefin composite material of the present invention is made of the following raw materials in mass percentage: 31% of tea fine powder treated with silane coupling agent, 57% of polyethylene, 9% of maleic anhydride grafted polyethylene, and 0.6% of stearic acid %, PE wax 1.8% and antioxidant 0.6%.
[0051] A preparation method of tea polyolefin composite material, comprising the following steps:
[0052] Step 1: Process the tea leaves into 150-mesh fine powder with a mechanical mill; immerse the fine powder into a diluted solution of KH550 silane coupling agent with a weight concentration of 2.8%, and soak for 3.5 hours under stirring; filter and separate the soaked fine powder Solid, dried at 81°C for 32 hours to obtain agglomerate powder; then use a mechanical mill to break up the agglomerate powder, and then dry at 81°C to constant weight to obtain tea fine powder treated with silane coupling agent ;
[0053] Step 2, prepare tea fine powder, polyethylene, m...
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