A kind of preparation method of ring structure micro-nano fiber
A technology of micro-nano fiber and ring structure, which is applied in the fields of fiber treatment, fiber chemical characteristics, spinning solution preparation, etc., to achieve the effect of expanding the application range, simple preparation process, and not easy to lose charge
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[0013] The specific process of preparing ring-shaped micro-nano fibers in this embodiment is as follows:
[0014] (1), preparing electrospinning solution: by weight percentage, be 10~12wt% polyvinyl alcohol PVA, the cerium nitrate of 1.5~2.5wt%, 88.5~85.5wt% deionized water preparation spinning solution, three according to above-mentioned The ratio is placed in an Erlenmeyer flask and sealed, magnetically stirred for 2 hours under heating in a water bath at 64 degrees Celsius, and then left to stand for 1 hour to obtain a uniform and transparent cerium nitrate / polyvinyl alcohol electrospinning solution;
[0015] (2), prepare cerium nitrate / polyvinyl alcohol micro-nano fibers under different voltages: connect the spinning nozzle 2 to the positive pole of the high-voltage electrostatic generator 3, and the metal collecting device 4 with adjustable area is connected to the negative pole of the high-voltage electrostatic generator 3, The prepared cerium nitrate / polyvinyl alcohol e...
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