Production method for preparing monocalcium phosphate and byproduct special fertilizer for capsicum annuum
A technology of calcium dihydrogen phosphate and calcium hydrogen phosphate, which is applied in the direction of chemical instruments and methods, applications, phosphorus compounds, etc., can solve the problems of increasing the production cost of calcium dihydrogen phosphate products, compaction of soil structure, difficulty in conformity, etc., to achieve Significant environmental value and economic benefits, cost reduction, and the effect of ensuring absorption efficiency
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Embodiment 1
[0044] A production method for preparing calcium dihydrogen phosphate byproduct capsicum special fertilizer, comprising the following steps:
[0045] (1) Preparation and mixing of raw materials: Phosphoric acid and carbonamide are placed in a stirred reactor at a molar ratio of 1.2:1, at a temperature of 80°C, and the stirring speed of the stirred tank is controlled at 180r / min to stir and mix for 2 hours to obtain an intermediate slurry;
[0046] (2) Preparation of calcium hydrogen phosphate: Add soluble calcium salt into the reaction kettle containing the intermediate slurry prepared in step 1) at a constant speed for 2 hours, control the pH value to 3, continue stirring and reacting for 10 minutes, and the reaction ends to obtain Slurry containing calcium hydrogen phosphate;
[0047] (3) Cyclic crystallization and filtration: place the slurry containing calcium hydrogen phosphate obtained in step 2) in a cooling crystallizer to cool down to a temperature of 20°C within 15s...
Embodiment 2
[0053] A production method for preparing calcium dihydrogen phosphate byproduct capsicum special fertilizer, comprising the following steps:
[0054] (1) Preparation and mixing of raw materials: Phosphoric acid and carbonamide are mixed in a stirred reactor at a molar ratio of 2.4:1, at a temperature of 100°C, and the stirring speed of the stirred tank is controlled at 200r / min to stir and mix for 3 hours to obtain an intermediate slurry;
[0055] (2) Preparation of calcium hydrogen phosphate: Add soluble calcium salt 3h at a constant speed to the reaction kettle containing the intermediate slurry obtained in step 1), control the pH value to 3.5, continue stirring and reacting for 15min, and the reaction ends to obtain Slurry containing calcium hydrogen phosphate;
[0056] (3) Cyclic crystallization filtration: place the slurry containing calcium hydrogen phosphate obtained in step 2) in a cooling crystallizer to cool down to a temperature of 18°C within 15s, cool down to c...
Embodiment 3
[0062] A production method for preparing calcium dihydrogen phosphate byproduct capsicum special fertilizer, comprising the following steps:
[0063] (1) Preparation and mixing of raw materials: Put phosphoric acid and carbonamide at a molar ratio of 1.8:1 in a stirred reactor at a temperature of 90°C and control the stirring speed of the stirred tank at 190r / min to stir and mix for 2.5 hours to obtain intermediate body slurry;
[0064] (2) Preparation of calcium hydrogen phosphate: Add soluble calcium salt into the reaction kettle containing the intermediate slurry obtained in step 1) at a constant speed for 2.5 hours, control the pH value to 3.3, continue stirring and reacting for 12 minutes, and the reaction ends. Obtain the slurry containing calcium hydrogen phosphate;
[0065] (3) Cyclic crystallization and filtration: place the slurry containing calcium hydrogen phosphate obtained in step 2) in a cooling crystallizer to cool down to a temperature of 19°C within 15s, coo...
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