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Normal-temperature thick-film zinc phosphide phosphating solution and experimental method for determining component proportions

An experimental method, zinc phosphide technology, applied in the coating process of metal materials, etc., can solve the problems of high-temperature phosphating solution cost, poor corrosion resistance, thin film thickness, etc., and achieve small porosity and corrosion resistance Good performance and low film forming temperature

Inactive Publication Date: 2015-01-07
SOUTHWEST PETROLEUM UNIV
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  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

[0003] The purpose of the embodiments of the present invention is to provide a normal-temperature thick-film zinc phosphide phosphating solution and an experimental method for determining the proportion of components, aiming at solving the problem of high-temperature phosphating solution cost, high energy consumption, and low-temperature phosphating solution film thickness. Thin, loose film formation, poor corrosion resistance

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  • Normal-temperature thick-film zinc phosphide phosphating solution and experimental method for determining component proportions
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  • Normal-temperature thick-film zinc phosphide phosphating solution and experimental method for determining component proportions

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Embodiment Construction

[0044] In order to make the object, technical solution and advantages of the present invention more clear, the present invention will be further described in detail below in conjunction with the examples. It should be understood that the specific embodiments described here are only used to explain the present invention, not to limit the present invention.

[0045] The application principle of the present invention will be further described below in conjunction with the accompanying drawings and specific embodiments.

[0046] The zinc-based phosphating solution of the normal temperature thick film phosphating of the embodiment of the present invention comprises: Zn(H 2 PO 4 ) 2 70g / L, Zn(NO 3 ) 2 100g / L, NaNO 2 0.6g / L, Ni(NO 3 ) 2 6g / L, Ce(NO 3 ) 3 .6(H 2 O) 10g / L, citric acid 1.5g / L, OP emulsifier 1ml / L, time 20min.

[0047] The preparation method of the solution: put 2 / 3 of the total volume of distilled water in a one-liter beaker, first add 1.5g of citric acid, st...

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Abstract

The invention discloses a normal-temperature thick-film zinc phosphide phosphating solution and an experimental method for determining component proportions. The normal-temperature thick-film zinc phosphide phosphating solution comprises 270g / L of Zn(H2PO4), 100g / L of Zn(NO3)2, 0.6g / L of NaNO2, 6g / L of Ni(NO3)2, 10g / L of Ce(NO3)3.6(H2O), 1.5g / L of citric acid, and 1ml / L of an OP emulsifier, wherein the time is 20 minutes; the experimental method for determining component proportions of the normal-temperature thick-film zinc phosphide phosphating solution comprises the following steps: preparing a solution; preparing a phosphating film; and testing performances. Due to the normal-temperature thick-film zinc phosphide phosphating solution comprising the components, the formed phosphating film is dark grey and free of hanging ash; the film is even and continuous and has complete coverage; the relationship between film weight and film thickness is about 1 to 1; the average film weight exceeds 18.13g / L; the obtained phosphating film is a heavy film and is mainly used for preventing stored spare parts from being corroded; and the phosphating film is fine in crystals, small in porosity, good in corrosion resistance, and excellent in film corrosion resistance.

Description

technical field [0001] The invention belongs to the technical field of zinc-based phosphating solutions, in particular to a normal-temperature thick-film zinc-based phosphating solution and an experimental method for determining component ratios. Background technique [0002] Phosphating treatment can be widely used in various industries, such as automobiles, machinery, shipbuilding, home appliances, military industry, aviation, etc. After years of development, phosphating technology has made many new achievements. In particular, the scope of application of phosphating has been greatly expanded, and phosphating has become an indispensable and important technology for steel processing, anti-corrosion, and decoration. In many chemical surface conversion treatment processes, phosphating treatment occupies a very important position. However, the traditional phosphating solution has high temperature, high energy consumption, and high cost. Although some phosphating solutions ha...

Claims

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Application Information

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IPC IPC(8): C23C22/17C23C22/77
CPCC23C22/17C23C22/77
Inventor 刘丽任呈强彭晔余嘉
Owner SOUTHWEST PETROLEUM UNIV
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