A kind of high transparency solid glue stick and preparation method thereof
A solid glue stick, transparency technology, applied in adhesives, non-polymer adhesive additives, N-vinylpyrrolidone copolymer adhesives, etc. Potential safety hazards of personnel and workshop environment, difficulty in large-scale production, etc., to achieve the effect of easy access to raw materials, low production costs, and easy control of reactions
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[0028] A preparation method for a high-transparency solid glue stick: it is characterized in that it comprises the following steps:
[0029] Step 1, prepare raw materials;
[0030] Step 2: Add the solvent into the reaction kettle, slowly add polyvinylpyrrolidone after stirring, dissolve at room temperature for 10 minutes to 60 minutes, then raise the temperature to 56°C to 88°C and then keep the temperature;
[0031] Step 3: Add excipients into the reaction kettle, and stir at constant temperature for 10 to 40 minutes until the excipients are completely melted and transparent and evenly dispersed in the solvent;
[0032] Step 4. Slowly add a pH regulator aqueous solution to the reaction kettle to adjust the pH value of the system to 10 to 12, and stir at a constant temperature for 10 to 50 minutes until the solution is transparent; after it becomes transparent, there is no white turbidity;
[0033] Step 5. Add a transparent agent into the reaction kettle, stir at a constant t...
Embodiment 1
[0036] Step 1, prepare raw materials according to the following weight percentages:
[0037] Polyvinylpyrrolidone 5%
[0039] Propylene Glycol 10%
[0040] Excipients: stearic acid 10%
[0041] pH adjuster: sodium hydroxide 1.5%
[0042] Potassium hydroxide 0.8%
[0043] Transparent agent: 10% ethanol
[0044] Sucrose 3%
[0045] The rest is water.
[0046] Step 2. Add the solvent (a mixture of 50% glycerol and 10% propylene glycol) into the reaction kettle, slowly add 5% polyvinylpyrrolidone after stirring, dissolve at room temperature for 10 minutes to 60 minutes, and then heat up to 56°C to 88°C Constant temperature after ℃;
[0047] Step 3: Add excipients (10% stearic acid) into the reaction kettle, stir at constant temperature for 10 to 40 minutes until the excipients are completely melted and transparent and evenly dispersed in the solvent;
[0048] Step 4. Slowly add a pH adjuster (a mixture of 1.5% sodium hydroxide and 0.8% potas...
Embodiment 2
[0052] Step 1, prepare raw materials according to the following weight percentages:
[0053] Polyvinylpyrrolidone 10%
[0055] Ethylene glycol 15%
[0056] Excipients: stearic acid 8%
[0057] Lauric acid 3%
[0058] pH adjuster: sodium hydroxide 2%
[0059] Potassium hydroxide 1%
[0060] Transparent agent: 15% ethanol
[0061] Sorbitol 5%
[0062] The rest is water.
[0063] Step 2. Add the solvent (a mixture of 30% glycerol and 15% ethylene glycol) into the reaction kettle, slowly add 10% polyvinylpyrrolidone after stirring, dissolve at room temperature for 10 minutes to 60 minutes, and then heat up to 56°C Constant temperature after reaching 88°C;
[0064] Step 3. Add excipient (a mixture of 8% stearic acid and 3% lauric acid) into the reaction kettle, stir at constant temperature for 10 minutes to 40 minutes until the excipient is completely melted and transparent and evenly dispersed in the solvent;
[0065] Step 4. Slowly add an ...
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