A kind of sludge treatment method
A sludge treatment and mixed sludge technology, applied in water/sludge/sewage treatment, oxidation treatment of sludge, metallurgical wastewater treatment, etc., can solve problems such as urban environmental pollution
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Embodiment 1
[0074] Use 1# municipal sludge raw material 95%, 3# steel mill sludge raw material 5%, oxidant is O 2 After grinding, add compounding agent (a mixture of lignosulfonate and humate, the addition ratio is 1:0.5, and the addition amount is 0.5wt‰) to the sludge to make its concentration reach 7%, and control the temperature of the reaction system The temperature is 580°C, the reaction pressure is 22MPa, the residence time of the mixed sludge of municipal sludge and steel mill sludge in the first high-pressure gas-liquid separator is 15min, and the outlet product at the upper end of the first high-pressure gas-liquid separator is decompressed CO, N are obtained after valve decompression 2 、CH 4 and other mixed gases, which contain a small amount of CO 2 Gas, the product at the outlet of the lower end of the first high-pressure gas-liquid separator enters the second high-pressure gas-liquid separator, and the product at the upper end is decompressed by a pressure reducing valve t...
Embodiment 2-8
[0076] For the specific process of Examples 2-8, see Example 1, and for the relevant parameters in each example, see Tables 4-5.
[0077] Table 4 Examples 1-4
[0078]
[0079] Note: COD* is chemical oxygen demand; municipal sludge and steel mill sludge are allocated according to percentage, totaling 100%.
Embodiment 5-8
[0082] Note: COD* is chemical oxygen demand; municipal sludge and steel mill sludge are allocated according to percentage, totaling 100%.
[0083] It can be seen from the above that the sludge treatment method provided by the embodiment of the present invention can make the mixed sludge react with the oxidant in supercritical water to be completely decomposed, and generate CO 2 Gas and slag water rich in metal oxides. This method can not only treat CO 2 The realization of resource utilization can also effectively transform the N, S, and P elements in the organic matter, and realize harmless treatment. At the same time, since steel mill sludge contains a large amount of transition metal elements, it plays a role in catalytic oxidation under the action of supercritical water oxidation, and also realizes the enrichment of transition metal elements, which is especially beneficial to the sludge containing heavy metal elements. Harmless treatment in the later stage to reduc...
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