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Novel efficient environment-friendly catalyst for regeneration of used oil

A waste oil and catalyst technology, applied in molecular sieve catalysts, physical/chemical process catalysts, chemical instruments and methods, etc., can solve problems such as loss of components and environmental pollution, and achieve the effect of ensuring safety, reducing pollution, and brightening the color.

Inactive Publication Date: 2015-04-01
郭帅
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If you continue to generate high-quality fuel oil, you need acid-base treatment, but as we all know, acid-base treatment will consume a considerable part of the oil, and the resulting acid residue and alkali residue will cause serious pollution to the environment, which is a national decree Prohibited behavior, this is a common problem of domestic small oil refineries

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Example 1: A new type of waste engine oil regeneration high-efficiency environmental protection catalyst, which includes the following steps:

[0025] Step 1: Carrier, main catalyst, co-catalyst, co-catalyst for ion exchange;

[0026] Step 2: Washing, filtering and drying;

[0027] Step 3: Forming;

[0028] Step 4: Roasting to form a finished catalyst;

[0029] Among them, the carrier in step 1 is ZSM-5 zeolite, Y zeolite and small pore Al 2 O 3, The main catalyst is Fe in the synthesis of NH3, the cocatalyst is K2O in the synthesis of NH3, and the co-catalyst is petroleum cracking SiO2-Al2O3; the ion exchange step is: weigh 50 grams of the carrier on the balance and put it into a three-necked flask, and the amount is simple Take the pre-prepared 1mol / LNH 4 Pour 500 mL of Cl solution into a three-necked flask, then put the three-necked flask into an electric heating bowl, and install a reflux condenser, stirrer, mercury thermometer on the electric heating bowl, and turn on the c...

Embodiment 2

[0033] Example 2: A new type of waste engine oil regeneration high-efficiency environmentally friendly catalyst, which includes the following steps:

[0034] Step 1: Carrier, main catalyst, co-catalyst, co-catalyst for ion exchange;

[0035] Step 2: Washing, filtering and drying;

[0036] Step 3: Forming;

[0037] Step 4: Roasting to form a finished catalyst;

[0038] Among them, the carrier in step 1 is ZSM-5 zeolite, Y zeolite and small pore Al 2 O 3, The main catalyst is Fe in the synthesis of NH3, the co-catalyst is K2O in the synthesis of NH3, and the co-catalyst is petroleum cracking SiO2-Al2O3; the ion exchange step is: weigh 50 grams of the carrier on a balance and put it into a three-necked flask. Take the pre-prepared 1mol / LNH 4 Pour 500 mL of Cl solution into a three-necked flask, then put the three-necked flask into an electric heating bowl, and install a reflux condenser, stirrer, mercury thermometer on the electric heating bowl, and turn on the cooling water, start the st...

Embodiment 3

[0042] Example 3: A new type of waste engine oil regeneration high-efficiency environmental protection catalyst, which includes the following steps:

[0043] Step 1: Carrier, main catalyst, co-catalyst, co-catalyst for ion exchange;

[0044] Step 2: Washing, filtering and drying;

[0045] Step 3: Forming;

[0046] Step 4: Roasting to form a finished catalyst;

[0047] Among them, the carrier in step 1 is ZSM-5 zeolite, Y zeolite and small pore Al 2 O 3, The main catalyst is Fe in the synthesis of NH3, the co-catalyst is K2O in the synthesis of NH3, and the co-catalyst is petroleum cracking SiO2-Al2O3; the ion exchange step is: weigh 50 grams of the carrier on a balance and put it into a three-necked flask. Take the pre-prepared 1mol / LNH 4 Pour 500 mL of Cl solution into a three-necked flask, then put the three-necked flask into an electric heating bowl, and install a reflux condenser, stirrer, mercury thermometer on the electric heating bowl, and turn on the cooling water, start the st...

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Abstract

The invention discloses a novel efficient environment-friendly catalyst for regeneration of used oil. The catalyst is prepared by the following steps: 1, performing ion exchange by using a carrier, a main catalyst, an auxiliary catalyst and a cocatalyst; 2, washing, filtering and drying; 3, forming; and 4, roasting to form a finished product catalyst. The catalyst has the following advantages: (1) the quality of produced oil can be obviously improved; (2) the selectivity to a product diesel oil is high, and the cetane value of the product diesel oil is relatively high, generally is 10-20 units higher than that of catalytic cracking diesel oil; and (3) the safety and catalytic effect are ensured under the condition that the space velocity is ensured to be appropriate, tail oil is ensured to be completely cracked when the used oil is treated from head oil to the end of oil refining, an engine oil component showing a green head is absolutely avoided, moreover, the produced oil does not have a peculiar smell, is clear and not muddy in color, and is close to water white to light yellow, the oil product quality is close to a national standard, the produced oil serves as a diesel engine fuel, the discharged tail gas accords with a corresponding national standard, and the pollution to the atmosphere is greatly reduced.

Description

Technical field [0001] The invention belongs to the technical field of energy regeneration and utilization, in particular to a new type of waste engine oil regeneration high-efficiency environmental protection catalyst. Background technique [0002] The petroleum refining industry is an important basic industrial sector of the national economy. It mainly provides various fuels (such as gasoline, diesel, etc.) for social production, and at the same time provides basic raw materials (such as benzene, phenol, etc.) for the chemical industry. Refining catalyst is an indispensable material used in petroleum refining industry. Since there are a large number of chemical reactions in the petroleum refining process, and the catalyst can change the chemical reaction rate and shorten the reaction time, its performance is directly related to the economic benefits of the petroleum refining industry. On the other hand, because the catalyst can also ease the reaction conditions, the petroleum ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J29/80C10G29/16
CPCY02A50/20
Inventor 郭帅
Owner 郭帅
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