Nano iron-carbon composite powder preparation method

A technology of carbon composite powder and nano-iron, which is applied in the direction of nanotechnology, nanotechnology, nanostructure manufacturing, etc., can solve the problems of unsuitability for industrial production, high requirements for reaction conditions, complex equipment, etc., and achieve low cost, simple equipment, The effect of lowering the reduction reaction temperature

Active Publication Date: 2015-04-08
山东鲁银新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Some of the above methods require high reaction conditions, complex equipment, difficult control, low yields,

Method used

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  • Nano iron-carbon composite powder preparation method

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Weigh 0.025 moles of ferric nitrate, 0.06 moles of glycine (reducing agent), and 0.04 moles of glucose (carbon source), dissolve various raw materials in deionized water, and prepare a solution; the solution is placed on a temperature-controllable electric furnace for heating, and the solution After a series of reactions such as volatilization, concentration, and decomposition, the precursor powder is obtained; in a hydrogen atmosphere, the precursor powder is placed in a furnace at 300°C for 2 hours to obtain a nano-iron-carbon composite powder.

Embodiment 2

[0027] Weigh 0.025 moles of ferric nitrate, 0.075 moles of glycine (reducing agent), and 0.05 moles of glucose (carbon source), dissolve various raw materials in deionized water, and prepare a solution; the solution is placed on a temperature-controllable electric furnace for heating, and the solution After a series of reactions such as volatilization, concentration, and decomposition, the precursor powder is obtained; in a hydrogen atmosphere, the precursor powder is placed in a furnace at 400°C for 2 hours to obtain a nano-iron-carbon composite powder.

Embodiment 3

[0029] Weigh 0.025 moles of ferric nitrate, 0.05 moles of alanine (reducing agent), and 0.04 moles of maltose (carbon source), dissolve various raw materials in deionized water, and prepare a solution; place the solution on a temperature-controllable electric furnace for heating , After the solution undergoes a series of reactions such as volatilization, concentration, and decomposition, the precursor powder is obtained; in a hydrogen atmosphere, the precursor powder is placed in a furnace at 500°C for 2 hours to obtain a nano-iron-carbon composite powder.

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Abstract

The invention belongs to the technical field of nano composite preparation and relates to a nano iron-carbon composite powder preparation method. The nano iron-carbon composite powder preparation method is characterized by including the steps: taking ferric nitrate as an iron source, taking water-soluble organics as a carbon source, and preparing the ferric nitrate, the carbon source and a reducing agent into homogeneous aqueous solution; heating the solution to enable volatilization, concentration and decomposition of the solution to obtain a precursor; calcining in a reducing atmosphere to obtain nano iron-carbon composite powder, wherein metal iron particles of the nano iron-carbon composite powder are uniform and adjustable in size distribution, iron/carbon phases of the nano iron-carbon composite powder are uniform in distribution and adjustable in content, and iron particles of the prepared nano iron-carbon composite powder are smaller than 20nm. The nano iron-carbon composite powder preparation method has the advantages of easiness in material acquisition, equipment simplicity, short process, high efficiency, low cost and applicability to industrial production.

Description

technical field [0001] The invention belongs to the technical field of nanocomposite material preparation, and in particular relates to a method for preparing nanometer iron-carbon composite powder. The method has simple equipment, short process flow, high efficiency and low cost, and is suitable for industrial production. technical background [0002] Nano-iron-carbon composite powder is a new type of multifunctional material uniformly compounded by nano-metal iron particles and carbon. Because the carbon layer is compounded around the nano-iron particles, the oxidation resistance and thermal stability of the nano-metal particles are improved, so that they can exist stably in the air for a long time, and the instability problem of the nano-metal iron particles is solved. Nano-iron-carbon composite powder not only has many excellent properties of nano-iron and carbon, but also has some new unique properties, so it shows great development potential and broad application prosp...

Claims

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Application Information

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IPC IPC(8): B82B3/00B82Y40/00
Inventor 秦明礼黄敏曲选辉曹知勤刘烨贾宝瑞陈鹏起吴昊阳李睿鲁慧峰
Owner 山东鲁银新材料科技有限公司
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