a fusion antigen protein
A technology for fusing antigens and proteins, applied in the direction of hybrid peptides, oxidoreductases, enzymes, etc., can solve the problems of insufficient specificity, low efficiency, long time, at least 6 hours, or even overnight reactions
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Embodiment 1
[0030] Gene fusion and expression
[0031] (1) Main reagents and equipment
[0032] PCR kits (including Taq enzyme, buffer, dNTP, T4 ligase) and DNA markers were purchased from full gold; protein markers were purchased from Beyond Biotech; BamH I, Xho I, EcoR I, Nco I, HindⅢ and other restriction internal Dicer was purchased from Takara (Dalian Bao Biology); calf intestinal alkaline phosphatase (CIAP) kit (including components: calf intestinal alkaline phosphatase, alkaline phosphatase buffer) was purchased from TaKaRa; gel recovery reagent Kits and plasmid extraction kits were purchased from OMEGA; kanamycin and ampicillin were purchased from BBI; IPTG was purchased from BBI; PCR primers and recombinant plasmid sequencing were completed by BGI or Invitrogen; other reagents were provided by Shenzhen New Industry Biomedical Engineering Co., Ltd. Inc. provided.
[0033]The ABI Veriti PCR instrument was purchased from ABI, the horizontal electrophoresis instrument RDY-SP1Z w...
Embodiment 2
[0054] Determination of the sensitivity and specificity of the antigenic protein expressed by the above insect cells to its corresponding antibody
[0055] The principle of the chemiluminescent immune sandwich method: the serum sample to be tested, the buffer solution and the antigen-coated magnetic microspheres are added to the reaction cup for reaction, and at 37°C, the antibody in the serum sample to be tested and the antigen coated on the magnetic microspheres are immune In the case of a magnetic field, the nano-magnetic beads will be magnetized rapidly, and the complex will be washed to obtain the complex of the antigen and the antibody to be tested. Other components will be washed away, and then the labeled protein A-NHS-ABEI will be added. Protein A can Quickly and specifically bind to the C-terminus of the antibody to be tested to form a "sandwich" immune complex. When the detected antibody content in the serum sample is more, the relative light intensity RLU detected ...
Embodiment 3
[0088] Comparison of prokaryotic and eukaryotic expressed proteins for detection of type 1 diabetes
[0089] hIA-2 and its truncated forms were expressed in Escherichia coli, and the optimized segment of hIA-2 screened above was respectively connected to the pGEX4T-1 expression vector, and the expression strain of Escherichia coli was BL21(DE3). After the expression product is purified by GST tag, the GST tag is cut off with Thrombin, and the untagged target protein is obtained by affinity chromatography.
[0090] The sensitivity and specificity of prokaryotic expressed hIA-2 to hIA-2 antibody were determined.
[0091] The prokaryotic expression segments of hGAD65 and its truncated forms are numbered PA1, PB1, PG1, and PH1 in sequence, corresponding to A1, B1, G1, and H1 expressed in eukaryotes.
[0092] The truncated prokaryotic expression segment of hIA-2- has a sign bit PN2, which corresponds to N2 in eukaryotic expression.
[0093] The detection platform and scheme detai...
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