High-capacity graphite composite material of lithium-ion battery and preparation method of composite material
A lithium-ion battery and composite material technology, which is applied in the field of high-capacity graphite composite materials for lithium-ion batteries and its preparation, can solve the problems of high-current charging and discharging performance and poor compaction performance of graphite, and achieve high-current charging and discharging performance. , Facilitate wetting and improve compatibility
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[0023] Example 1:
[0024] A high-power electrode material with a graphitization degree of about 94% is selected and mechanically crushed into 16um particles to obtain highly graphitized particles.
[0025] Put natural graphite particles (D5011um) 222.5kg, coal tar pitch (D5010um) 25kg and graphitization catalyst SiC 2.5kg into the drum furnace. When feeding, the drum is rotating while feeding, and heating and kneading are performed after feeding. Adjust the rotating speed of the drum to 30Hz, and the heating program is: normal temperature to 200°C for 1 hour, 200°C to 400°C for 3 hours, 400°C to 600°C for 3 hours, and 600°C constant temperature for 2 hours. Cool to room temperature. The secondary composite particles (D5016.0um) with core-shell structure were prepared.
[0026] Put 10kg of the above highly graphitized particles, 89kg of core-shell structured secondary composite particles, and 1kg of coal pitch (D508um) into the reactor. When feeding, add while stirring, and heat af...
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[0028] Example 2:
[0029] The crucible material with a graphitization degree of about 93% is selected, and the highly graphitized particles are made by mechanical crushing into 17um particles.
[0030] Put 225kg of natural graphite particles (D5010um), 26kg of coal pitch (D5010um), and 2.8kg of graphitization catalyst SiC into the drum furnace. When feeding, the drum rotates while feeding, and heating and kneading are performed after feeding. Adjust the rotating speed of the drum to 30Hz, and the heating program is: normal temperature to 200°C for 1.5 hours, 200°C to 400°C for 3 hours, 400°C to 600°C for 3.5 hours, and 600°C constant temperature for 3 hours. Cool to normal temperature to prepare secondary composite particles with core-shell structure.
[0031] Put 30kg of the above highly graphitized particles, 69kg of secondary composite particles with core-shell structure, and 1kg of coal pitch (D508um) into the reactor. When feeding, add while stirring, and heat after feeding. ...
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