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Method for preparing conductive composite material

A conductive composite material, high temperature furnace technology, used in fibrous fillers, dyeing low molecular organic compound treatment, dyeing physical treatment and other directions, can solve the problems of high addition amount of conductive properties, achieve good mechanical properties and electromagnetic shielding properties, easy to use. Operation, wire can be good effect

Inactive Publication Date: 2015-05-20
龙继东
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although there are also some reports on carbon black and graphite filled polymers, because the fillers are at the micron level, the percolation threshold is generally between 15% and 20%, so a higher amount of addition is required to obtain better electrical conductivity.

Method used

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Experimental program
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Embodiment Construction

[0014] A kind of preparation method of conductive composite material, it is characterized in that comprising the steps:

[0015] (1) Expand the expandable graphite in a high-temperature furnace at 950°C to obtain EG; configure a saturated ethanol solution of sodium oleate, pour EG into a beaker, and add sodium oleate / ethanol solution;

[0016] (2) Then heat and stir the beaker on a magnetic stirrer for 0.5h; after stirring, ultrasonically shake the beaker in a water bath for 2.5h;

[0017] (3) Finally, the GNP obtained by ultrasonic pulverization is suction-filtered and dried in a drying oven;

[0018] (4) Take 90 parts of PP and 10 parts of POE to form the matrix resin, add 20 parts of GNP into it; stir in a high-speed mixer, extrude and granulate through a twin-screw granulator to complete the preparation of conductive composite materials.

[0019] In the preparation method of a conductive composite material described in the present invention, the mass concentration of the ...

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PUM

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Abstract

The invention relates to a method for preparing a conductive composite material and belongs to the field of preparation of materials. The method is characterized by comprising the following steps of placing expandable graphite in a high-temperature furnace and puffing to obtain EG; pouring the EG into a beaker and adding an sodium oleate / ethanol solution; placing the beaker on a magnetic stirrer, heating and stirring; after the stirring, carrying out ultrasonic vibration on the beaker in a water bath; and finally, carrying out suction filtration on GNP prepared by ultrasonic pulverizing and drying in a drying box; adding GNP into matrix resin comprising PP and POE; stirring in a high-speed mixer, and extruding and granulating by virtue of a twin-screw granulating machine group to complete the preparation of the conductive composite material. The content of graphite nanosheets is improved so that the prepared conductive composite material has good conductivity, better mechanical properties and electromagnetic shielding property. The method of the conductive material is simple in process and is easy to operate and the conductive material has larger market value.

Description

Technical field [0001] The present invention is a material preparation field, especially the preparation method of conductive composite materials. Background technique [0002] With the continuous progress of technology, material technology has developed rapidly, and high -molecular conductive composite materials can be used for the electrode, anticorrosive coating, electromagnetic shielding of fuel cells. In order to improve the conductive performance of the materials, metal particles, charcoal black, graphite powder are added to be addedWait for conductive fillers.The conductive performance of the polymer conductive composite material depends on the particle size of the conductive filler, the surface area of the comparison, and the orientation of the particles during processing.People expect to obtain high conductive performance with smaller fillers, that is, the material has a lower filtration threshold, which is conducive to the molding processing of the material.Therefore, s...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/12C08L23/08C08K9/04C08K7/24C09C1/46C09C3/08C09C3/04
CPCC08L23/12C08K2201/001
Inventor 龙继东
Owner 龙继东
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