Disperse dye compound as well as preparation method and use of disperse dye compound
A technology of disperse dyes and compounds, applied in acylation preparation, dyeing method, organic chemistry, etc., can solve the problems of low tinting strength, low affinity, easy entry and exit, etc., to improve affinity, increase van der Waals force, and increase contact face effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0026] Add 1.00g of purified and vacuum-dried C.I. Disperse Blue 106 dye to a 500ml three-necked flask, add an appropriate amount of dehydrated 300ml of dichloromethane as a solvent, stir to completely dissolve the disperse dye, add 0.61g for dehydration Accurately weigh 0.40g of diformyl chloride compound, dissolve and dilute it with an appropriate amount of reaction solvent, slowly drop it into a stirred reactor in an ice bath, and raise the temperature to room temperature for 2-4h. TLC spotting to trace the reaction process, after the reaction is completed, add 100ml of aqueous solution containing dilute acid, extract and separate, spin the dye solution to remove the dichloromethane solvent, then wash and filter with an appropriate amount of sodium carbonate solution, and wash with water to obtain 1.18g of crude product , and the yield was 84.29%.
[0027] The crude product is recrystallized from dimethylformamide to obtain the pure product of the novel disperse dye compoun...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com