A kind of ceramic diaphragm and its preparation method and application
A technology of ceramic diaphragm and ceramic particles, which is applied in the direction of structural parts, electrical components, battery pack parts, etc., can solve the problems of unusable and insufficient electrochemical performance of batteries, and achieve reduced influence, high crystallinity, and broadened selection range Effect
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[0024]The preparation method of the ceramic diaphragm provided by the present invention includes coating a slurry containing ceramic particles, a binder and high-density polyethylene on at least one side surface of the substrate and drying, and the particle size of the ceramic particles is not smaller than the specified The particle size of the above-mentioned high-density polyethylene, and the melting point of the high-density polyethylene is higher than 120°C.
[0025] Wherein, the specific types and contents of the ceramic particles, binder and high-density polyethylene have been described above, and will not be repeated here.
[0026] The binder is generally a polymer binder, therefore, in order to ensure its dispersibility in the slurry, the binder is preferably used in the form of a binder emulsion, and its solid content can be 30-60 weight%. In addition, in order to ensure the dispersibility in the slurry and ensure that it has a smaller particle size, the high-density...
Embodiment 1
[0035] This embodiment is used to illustrate the ceramic diaphragm provided by the present invention and its preparation method.
[0036] Add 0.045g of sodium polyacrylate (purchased from Shandong Taihe Water Treatment Co., Ltd., CAS No. 9003-04-7, the same below) and 1.2g of pure acrylic emulsion with a solid content of 50% by weight (purchased from Taihe Water Treatment Co., Ltd. From Guangdong Haishun New Material Technology Co., Ltd., brand HMP-2610, the same below), after stirring evenly, add 1.5g of aluminum oxide particles with a particle size of 400-500nm, stir at high speed, and then add 2.86g with a solid content of 35% by weight %, high-density polyethylene emulsion with a particle size of 50-100 nm (melting point is 135 ° C, purchased from Shanghai Xinnuo Chemical Co., Ltd.), and stirred evenly to obtain a slurry. Then the slurry is coated on the both sides of the PP separator (purchased from Huizhou Dewei Electronics Co., Ltd., model is 16-40, the same below) and ...
Embodiment 2
[0038] This embodiment is used to illustrate the ceramic diaphragm provided by the present invention and its preparation method.
[0039] Add 0.045g of polyethylene oxide (purchased from Guangzhou Liguo Trading Co., Ltd., CAS No. 25736-86-1) and 1.2g of styrene-acrylic emulsion with a solid content of 50% by weight (purchased from Shengda Chemical Co., Ltd. , grade S-01), after stirring evenly, add 1.5g of aluminum oxide particles with a particle size of 100-200nm, stir at high speed, and then add 2.5g of high-density Al2O3 particles with a solid content of 40% by weight and a particle size of 30-60nm Oxidized polyethylene (with a melting point of 137°C, purchased from Guangzhou Wanggao Chemical Co., Ltd., brand name A-C330) was stirred evenly to obtain a slurry. The slurry is then coated on both sides of the PP diaphragm and dried to obtain a ceramic diaphragm T2 comprising a base and a coating attached to both sides of the base, wherein the thickness of the base is 25 μm, an...
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