Three-dimensional hierarchical heterostructure nano-material, and gradient hydro-thermal preparation method and application thereof
A technology of heterostructures and nanomaterials, applied in nanotechnology, nanotechnology, structural parts, etc., can solve the problem of difficulty in obtaining three-dimensional heterostructured nanostructures, and achieve large specific surface area, reduced damage, and excellent electrochemical performance. Effect
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Embodiment 1
[0044] 1) Weigh 0.14g ammonium metavanadate and 0.25g citric acid monohydrate, add 35mL deionized water, stir for about one minute to form a uniform transparent yellow solution;
[0045] 2) Add 0.5 g of sodium lauryl sulfate to the solution in step 1), and magnetically stir it in a constant temperature water bath at 50° C. for 4 hours to dissolve it and form a transparent and uniform dark blue solution;
[0046] 3) Take out the precursor solution obtained in step 2) from the water bath and let it stand for 1 min, transfer it to a 50mL reaction kettle, and conduct a hydrothermal reaction in a constant temperature oven at 180°C for 24 hours;
[0047] 4) After the reaction kettle in step 3) is naturally cooled to room temperature, pour off the upper layer solution, obtain the black precipitate at the bottom, wash and centrifuge;
[0048] 5) drying the sample obtained in step 4) in a vacuum oven at 70°C for 6 hours;
[0049] 6) Calcining the dried sample in step 5) at a heating r...
Embodiment 2
[0058] 1) Weigh 0.14g ammonium metavanadate and 0.25g citric acid monohydrate, add 35mL deionized water, stir for about one minute to form a uniform transparent yellow solution;
[0059] 2) Add 0.1 g of sodium lauryl sulfate to the solution in step 1), and magnetically stir it in a constant temperature water bath at 50°C for 4 hours to dissolve it and form a transparent and uniform dark blue solution;
[0060] 3) Take out the precursor solution obtained in step 2) from the water bath and let it stand for 1 minute, transfer it to a 50mL reaction kettle, and conduct a hydrothermal reaction in a constant temperature oven at 180°C for 24 hours;
[0061] 4) After the reaction kettle in step 3) is naturally cooled to room temperature, pour off the upper layer solution, obtain the black precipitate at the bottom, wash and centrifuge;
[0062] 5) drying the sample obtained in step 4) in a vacuum oven at 70°C for 6 hours;
[0063] 6) Calcining the dried sample in step 5) at a heating ...
Embodiment 3
[0066] 1) Weigh 0.14g ammonium metavanadate and 0.25g citric acid monohydrate, add 35mL deionized water, stir for about one minute to form a uniform transparent yellow solution;
[0067] 2) Add 0.3 g of sodium lauryl sulfate to the solution in step 1), and magnetically stir it in a constant temperature water bath at 50° C. for 4 hours to dissolve it and form a transparent and uniform dark blue solution;
[0068] 3) Take out the precursor solution obtained in step 2) from the water bath and let it stand for 1 minute, transfer it to a 50mL reaction kettle, and conduct a hydrothermal reaction in a constant temperature oven at 180°C for 24 hours;
[0069] 4) After the reaction kettle in step 3) is naturally cooled to room temperature, pour off the upper layer solution, obtain the black precipitate at the bottom, wash and centrifuge;
[0070] 5) drying the sample obtained in step 4) in a vacuum oven at 70°C for 6 hours;
[0071] 6) Calcining the dried sample in step 5) at a heatin...
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