Base film, and laminated structure and display device comprising same
A technology of base film and conductive film, applied in identification devices, conductive layers and coatings on insulating carriers, etc., can solve the problems of low glass transition temperature, unsuitable for display field, polymer film modification, etc.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment and
[0083]
Embodiment 1
[0085] (1) Preparation of cycloolefin-based polymers
[0086] At room temperature, 5-norbornene-2-carboxylic acid butyl ester (100 g) with 71 mol% external isomer and 5-norbornene-2-carboxylic acid methyl ester with 71 mol% external isomer The ester (900 g) was placed in a reactor and toluene (3000 g) was added thereto. 1-Octyne (10.8 g) was further added thereto, and then the inside of the reactor was replaced with nitrogen, and the temperature of the reactor was raised to 105°C. Then, catalyst palladium acetate trimer (0.288 g) and tricyclohexylphosphonium tetrakis(pentafluorophenyl)borate (2.46 g) dissolved in methylene chloride were put into the reactor, followed by stirring for 18 hours to react. After 18 hours, a white polymer precipitate was obtained from the reaction using acetone and ethanol. The precipitate was filtered with a filter to obtain a polymer, which was dried in a vacuum oven at 60° C. for 24 hours to prepare butyl 5-norbornene-2-carboxylate and 5-norbo...
Embodiment 2
[0091] Except using butyl 5-norbornene-2-carboxylate (300 g) with 71 mol% exo isomer and methyl 5-norbornene-2-carboxylate (700 g ), and the use of 1-octyne (10.3g), palladium acetate trimer (0.275g) and tricyclohexylphosphonium tetrakis (pentafluorophenyl) borate (2.36g), by and Example 1 A copolymer of butyl 5-norbornene-2-carboxylate and methyl 5-norbornene-2-carboxylate was prepared in the same manner, and a base film including the copolymer was produced.
PUM
| Property | Measurement | Unit |
|---|---|---|
| glass transition temperature | aaaaa | aaaaa |
| thickness | aaaaa | aaaaa |
| glass transition temperature | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More 